Abstract. The cryptic gastropod species Nucella emarginata and Nucella ostrina are distributed along the northeastern Pacific coast from Alaska to Baja, California. N. emarginata is found primarily in the south and N. ostrina is found primarily in the north, with their ranges overlapping in central California. Snails (7- 34 individuals) from four locations in the overlap zone were collected and their population structures were studied using an approximately 500 bp fragment of the mitochondrial gene cytochrome c oxidase subunit I (COI). Contrary to what might be expected, analysis showed snails from the southern locations of Soberanes Point and San Luis Obispo are both N. ostrina (the northern species), while snails from the northern locations at Hopkins Marine Station in Pacific Grove and Point Joe are both N. emarginata. Although populations in each location are fairly homogenous, small amounts of variation do exist within each population (i.e. some polymorphisms are present). Of particular note is the variation that exists between snails collected from a wave exposed area at Hopkins Marine Station and snails in a wave protected area on the other side of the same point. Despite this intra- population variation, each location forms a genetically distinct group. Further sampling in central California will give more insight into the distribution of Nucella over short geographical distances and will hopefully elucidate more of these species’ evolutionary histories, as well as possibly helping to determine what factors are important in Nucella distribution. INTRODUCTION Isolation between species leads to speciation. This isolation can be the result of geographic barriers, as is the case with allopatric speciation. However, speciation can also occur in the absence of obvious physical barriers, especially in the marine environment (Palumbi 1992). Here, isolation is the result of genetic differentiation, which in turn leads to reproductive isolation. When species have large ranges, but low dispersing larvae, genetic differentiation should be seen between distant populations since gene flow between them will be small. This process is known as “isolation by distance“ and is generally intended to apply to continuously distributed populations (Wright 1943). In a similar model, the "stepping stone" model (Kimura and Weiss 1964), gene flow occurs between adjacent populations, but not between more distant ones. Both of these models predict a decrease in genetic correlation over long distances. Genetic differentiation over geographic distance has been observed along the Pacific coast of North America in several species, including copepods (Burton et al. 1979, Burton and Feldman 1981) and corals (Hellberg 1994, Hellberg 1995). In the case of corals, Hellberg (1995) has shown that the coral Balanophyllia elegans follows the stepping stone model over smaller spacial scales, but not at the rangewide level. Both of these models would lead to parapatric speciation, speciation in which some gene flow occurs (reviewed in Gavrilets et al. 2000). Taxa with low larval dispersal make good systems for studying patterns of speciation because they have higher rates of both speciation and extinction (Hellberg 1994). This study focuses on two sister species from the gastropod genus Nucella, the dog-whelks, as another model system for studying genetic differentiation over small geographic ranges. This system, however, is unique because two closely related, and recently diverged, species can be studied simultaneously in a range where their distributions overlap. Members of Nucella are found along the eastern Pacific coast from Alaska to Baja, California (Palmer et al. 1990, Marko 1998). Due to extreme morphological similarities between these species, they have had a confused taxonomic history. Most recently, Palmer et al. (1990) showed that the "species" N. emarginata was in fact two cryptic species. The southern populations retained the name N. emarginata and the northern populations became N. ostrina. Since then, considerable effort has been spent trying to describe reproductive, morphological and genetic differences between these two species (Palmer et al. 1990, Marko 1998, Marko et al. 2003). N. emarginata and N. ostrina are fairly easy to distinguish by the shape of their egg cases, with N. emarginata eggs being shorter and fatter than those of N. ostrina (Palmer et al. 1990). In contrast, using shell morphology to distinguish between species tends to be quite difficult since several morphs exist within both species (Marko et al. 2003, Crothers 1984, personal observation). Palmer et al. (1990) and Marko et al. (2003) suggest that N. emarginata and N. ostrina can be differentiated by the number of body whorls, whether the spiral cords are knobby or continuous, the size of the aperture, and the presence of an adapical tooth on the columella. However, these traits are not always well defined and do not provide a reliable method for identifying the species. Genetic methods are also available to distinguish between N. emarginata and N. ostrina. Marko (1998) used both nuclear (allozyme) and mitochondrial DNA to identify Nucella species along the northeastern Pacific coast. His analysis showed that N. emarginata and N. ostrina are genetically distinct at nine allozyme loci. He additionally found twenty-five distinct mitochondrial DNA haplotypes. Using these molecular techniques, Marko found that N. ostrina is present from Alaska to central California, while N. emarginata is found from central California to Baja, California. There is a zone of overlap between the two species in central California. Marko further suggests that these two species diverged as the result of reproductive isolation caused by a biogeographic boundary, possibly at Point Conception. The current overlap of species in central California could then be the result of northward range expansion by N. emarginata. This study focuses on a closer examination of the distribution of Nucella in central California, from Pacific Grove to San Luis Obispo (approximately 240 km away). We examined the population structure by looking at cytochrome c oxidase subunit I (COl), a mitochondrial gene involved in the electron transport chain during respiration. COl is highly conserved across species, so variations within this locus can give insight into evolutionary relationships. Polymorphisms within this gene additionally provide a reliable method for distinguishing between N. emarginata and N. ostrina. The use of COI therefore allows the determination of the distribution of species along the central California coast. The genetic structure of these populations can be used to provide additional information about the evolutionary history of Nucella, as well helping to explain what causes the observed distribution. It can be tested whether sharp changes in genetic structure occur at biogeographic boundaries (see Avise 1992) or if there is some other physical boundary responsible for the shift. It would also be possible to determine if the distribution of Nucella in central California is dependent on other factors, such as temperature, salinity or wave exposure gradients. In the future, if shifts were observed in the range of either of these species, it could then be possible to relate these changes to climate change or to changes in other environmental factors. MATERIALS AND METHODS Sample collection and DNA extraction. Nucella species were collected at four different sites along the California coast between April 23 - May 24, 2003. At Hopkins Marine Station (HMS) in Pacific Grove (36°37’N, 121°54’W), thirteen snails were collected in the wave protected area near the pilings and twenty-one snails were collected in a wave exposed area. At Point Joe (JOE) (36°36’N, 121°57W2), six snails were collected in a wave exposed area, five snails were collected in an area with moderate wave exposure and two snails were collected in a wave protected area. At Soberanes Point (SÖB), eight snails were collected from a wave- exposed area near the USGS benchmark (36°22’30"N, 121°52’30“W). In San Luis Obispo (SLO) (35°20’N, 120°43’W), seven snails were collected in a wave protected area in St. Luis Harbor, near Pismo Beach. The shell morphology of snails was examined and shell coloration, shell texture, the number of whorls, angular vs. rounded "shoulder", and the presence of an adapical tooth were recorded. Snails were additionally photographed. Äfter the examination of shell morphology, snails were placed in an isotonic solution of magnesium chloride (MgCl) for 30- 60 minutes in order to relax their muscles. A snail was considered to be relaxed when it no longer withdrew into its shell when touched. A small piece of foot-tissue was then biopsied. Tissue was digested and DNA was extracted using the Nucleospin Tissue Kit (Machery- Nagel/BD Biosciences). PCR and Sequencing. A 463 bp fragment from the mitochondrial gene cytochrome c oxidase subunit I (COI) was amplified using the polymerase chain reaction (PCR). Several previously published COI primers were tried, including the universal primers COla and COlf (Palumbi), the universal primers 1490 and 2198 (Folmer 1994) and the Nucella canliculata COl primers COIM-L and COIM-H (Sanford 2003). These primers, for the most part, did not result in successful amplifications, so new primers were designed from published N. emarginata and N. ostrina sequences: Nucella COIF (S’-CTCATATTGTGRGCCATTATTCAGC-3’) and Nucella COIR (S’-CAACGACTATGAAGCGAAACACCC-32). DNA template (1 uL of a 1:100 dilution) was added to a reaction mix consisting of 16.4 uL ddH2O, 2.5 uL 1OX PCR buffer, 2.5 uL dNTPs (8 mM), 1.25 uL each primer (10 mM) and 0.3 uL AmpliTaq polymerase. The PCR profile consisted of a 2 min incubation at 94°C, followed by 36 cycles of 94 °C for 30 sec, 60 °C for 1 min, and 72 °C for 1.5 min. PCR products were visualized on 2% agarose gels stained with ethidium bromide. The products of successful PCR amplifications were then prepared for sequencing as follows: PCR product (5 uL) was added to 2 uL Shrimp Alkaline Phosphatase (SAP), 1 uL Exonuclease I (EXO) and 0.5 uL dilution buffer and then incubated at 37 °C for 30 min, followed by 80 °C for 15 min. This reaction removes excess dNTPs and primer dimers. SAP product (2 uL) was then added to 6 uL ddH2O, 1 uL Big Dye, 1.5 uL 5X buffer, and 0.5 uL primer (10 mM). This reaction mixture was then cycle sequenced for 25 cycles of 96°C for 10 sec, 50 °C for 5 sec, and 60 °C for 4 min in order to add fluorescent dye to the nucleotide bases. After cycle sequencing, DNA was precipitated with 40 uL of 75% isopropanol for 15 min and then pelleted by spinning at approximately 3200 rpm for 1 hour. Excess isopropanol was removed by inverting the opened tubes and spinning them at 700 rpm for 2 min. Samples were resuspended in 20 uL of High Dye, heated at 96 °C and then sequenced using an ABI3100 Genetic Analyzer. Analysis of sequences. Sequences were viewed using Sequencher"" 4.1. Both the sequence of bases and their corresponding chromatograms were examined and sections of sequence with unclear chromatograms (i.e. where obvious, individual peaks were not present) were removed. The forward primer and reverse primer sequences for each snail were compared and then combined into a single consensus sequence. These consensus sequences were aligned by assembling them into a contig and then were examined for polymorphisms, both within and -6- between populations. All sequences were additionally compared to published sequences for N. emarginata and N. ostrina (Genbank accession numbers AF076536-AF076560) to determine which species were present within a geographic location. Following the “cleaning" of sequences and the preliminary analysis using Sequencher"" 4.1, the consensus sequences were transferred to PAUP“4.Ob10 (PPC) to create phylogenetic trees based on a parsimony analysis. Consensus sequences were also analyzed using heap big Power Mac (program by S. Palumbi) to calculate variation within and among geographic locations, as well as the corresponding Fsr value. The Fsr value was calculated by dividing the variation within a population by the variation between the populations and subtracting this answer from one. A bootstrap analysis was then performed to calculate P-values. RESULTS Morphology. Shells from both N. emarginata and N. ostrina exhibited a wide range of morphologies (Fig. 1). Shell colors ranged from light (white, various shades of gray, and tan) to dark (black, brown, and maroon). Some shells additionally had stripes. Certain morphs of both species had smooth shells, but only N. emarginata exhibited a highly knobby shell. Both species had between four and six body whorls and could have either angular or rounded shoulders. The presence of an adapical tooth was only observed in N. emarginata. PCR and sequencing. Performing PCR with the universal primers 1490 and 2198 (Folmer) yielded no amplification products (Fig. 2). PCR with the universal primers COla and COIf (Palumbi) either yielded no amplification products or products with multiple bands (Fig. 3). PCR with the primers COIM-H and COIM-L (Sanford) yielded good amplifications about 55% of the time (Fig. 4), but the corresponding sequences contained ambiguous bases at several nucleotide sites. PCR with the new primers Nucella COIf and Nucella COIr yielded both clean amplifications and clean sequences (Fig. 5). Analysis of sequences. The 463 bp COI fragments from all four geographic locations had 12 variable sites, which resulted in 10 unique haplotypes (Table 1, Fig. 6). Comparisons of these haplotypes to published sequences for N. emarginata and N. ostrina show that the populations at Hopkins Marine Station and Point Joe are N. emarginata and the populations at Soberanes Point and San Luis Obispo are N. ostrina (Fig. 7). Four nucleotide base sites were used to make the determination between species. At each of these sites, all of the N. ostrina individuals had one base, while a majority of the N. emarginata individuals showed another base. All of the individuals in this study were polymorphic at these sites, however, a few of the previously published N. emarginata sequences (Marko 1998) did not share these polymorphisms (see appendix). The presence of a certain nucleotide base at each of these four nucleotide sites allowed for the positive identification of N. emarginata individuals, since these four bases are only observed in N. emarginata. The presence of the alternate base implies that the individual is an N. ostrina, however this assumption could possibly have led to misidentified individuals. To help identify individuals with a greater level of certainty, unmarked shells from Point Joe and San Luis Obispo were additionally sent to an expert for identification (Marko, pers. comm.). His species designations agreed with the species designations made based on sequences. This patchwork distribution of species is somewhat unexpected, since species often have continuous ranges. Not only is there variation between species, but variation within a population also exists. Intrapopulation variation ranged from 0.056 - 0.194%, while variation between populations of each species ranged from 0.218- 0.546%. These values give Fsr ratios between 0.303 and 0.852 (Table 2). Using these Fsr ratios to perform bootstrap analyses shows that all four geographic locations have genetically distinct populations (P + 0.0001 in all cases). Although significant, this variation is very small, with haplotypes of a species varying by no more than three nucleotide bases. The significance arises because these haplotypes are very local, with only one haplotype being observed in more than one geographic location (Table 1). Figures 8 and 9 show two parsimony trees generated by doing a heuristic search with branch-swapping and random stepwise addition. Figure 8 shows one of the one hundred trees generated. Figure 9 is the majority rules consensus tree for these same one hundred trees, i.e. this tree shows only branching that occurred in at least 50% of all trees. Since Hopkins Marine Station had the largest sample size, its population structure was examined more carefully. Three unique haplotypes are present at Hopkins Marine Station (Table 1). One haplotype clusters with N. ostrina on a phylogenetic tree, and differs from the other two haplotypes by at least seven nucleotide bases. The other haplotypes cluster with N. emarginata on a phylogenetic tree (Fig. 8) and differ from each other by only one nucleotide base. The observed polymorphism is a cytosine to guanine transversion, which is somewhat uncommon. It is possible that this transversion is due to sequencing error. However, the sequences showing the transversion were sequenced on different days and with different sets of primers, so the probability of this result being sequencing error is small. Looking only at the N. emarginata sequences at Hopkins Marine Station, differences in population structure are apparent between wave exposed and wave protected areas. The shift in haplotype frequencies between protected and exposed sites is significantly different (Fsr = 0.089, P = 0.03. See Fig. 10). These two sites are separated by approximately 100 m, including an approximately 10 m stretch of sand, which could have prevented members of these populations from reaching each other to reproduce. DISCUSSION Both N. emarginata and N. ostrina were found in central California, as expected based on previous work (Marko 1998, Marko 2003). Even though it is the southern of the two species, N. emarginata was found at the two northern sites at Hopkins Marine Station and Point Joe, while N. ostrina was found at the two southern sites at Soberanes Point and San Luis Obispo. A brief glance at the phylogenetic trees suggests, and the results of bootstrapping confirm, that all four of these locations are genetically distinct populations (P + 0.0001). This result is expected, since Nucella populations are very isolated from each other. Although low larval dispersal does not always lead to genetic differentiation over distance (McFadden and Aydin 1996), isolation between populations is also observed in other low dispersal species, including some copepods (Burton et al. 1979) and some corals (Hellberg 1994). Rather than releasing larvae into the ocean where they can be carried hundreds of kilometers away as many marine invertebrates do, Nucella lay egg cases in which the embryonic snails develop before emerging as juvenile snails. Individual snails then do not move very far during their lifetime (see West 1986 for snail movement over a 4 month period). Gene flow is thus very limited between separate populations and the genetic structure of a population is determined almost entirely by local egg production. Laboratory studies also show that little or no hybridization occurs between the two species (Marko, pers. comm.), which would further reduce the possibility of genetic mixing of populations. Each geographic location additionally only has one of the two species. However, there are two possible exceptions. First, one snail from Hopkins Marine Station (E7) clusters with the snails from Soberanes Point. It is possible that this individual is actually an N. emarginata with -10- N. ostrina-like sequence, in which case there would still only be one species present at Hopkins Marine Station. Or, if this individual is an N. ostrina, there could be a small population of N. ostrina at Hopkins Marine Station, with more individuals not being found due to the relatively small sample size (34 individuals). If this is the case, it would oppose the trend seen both in this study and by Marko (1998, pers. comm.) for only one species to be present per site. Another possibility is that a single N. ostrina made it to Hopkins Marine Station, possibly stuck to the side of a kayak, or brought accidentally by a researcher. Without other members of its species present, this snail will most likely die without reproducing, thus having no effect on the genetic structure of the Hopkins Marine Station population. The other possible exception involves San Luis Obispo. This study found only N. ostrina at San Luis Obispo; however, Marko (1998) found only N. emarginata there. Most likely, these two sample populations were collected from different areas, with each area having its own distinct population. If this is the case, the change in genetic structure occurs over a very short distance. However, the location at which Marko collected his snails is unavailable at this time, so it remains unknown as to whether these two species inhabit the same rocky headland. Overall, the trend seems to be that only one species is present per geographic location. Why would this be the case? One hypothesis is that this phenomenon is due basically to chance. Whichever species happens to colonize a location first (having gotten there by migration, or on floating debris or a boat, etc.) is able to dominate in resource use and prevent members of the other species from establishing a population. Such a founder event could also lead to a rapid shift in the genetic structure of a population, as it adapts to a new environment (Palumbi 1994). If this founder effect occurred, it would further help to explain the genetic distinctness observed at each geographic location. Another possibility is that selection might be acting on these two species. Previous work has shown that clines in physical -11- factors can correspond to clines in the allozymes responsible for dealing with these factors. Mitochondrial haplotypes often also follow this cline (reviewed in Palumbi 1994). If one species of Nucella is better adapted to certain environmental condition(s) in a particular location, natural selection could prevent the other species from being able to establish a population. It is then possible that the patterns observed in COI could be reflecting this selection. Genetic structure is evident over small geographic ranges in Nucella in central California. Further collection of snails in the zone of overlap between the two species will hopefully shed light on what is responsible for the distribution of each species - whether it is determined by an environmental gradient, or if physical barriers are the major factor, or if distribution is the result of random migration events in the past. Additional geographic locations would also allow the determination of whether Nucella species follow either the isolation by distance or stepping stone models. In order to examine these questions, more snails will be collected between Soberanes Point and San Luis Obispo at various distances apart to continue to determine the small-scale genetic structure of these two species. ACKNOWLEDGEMENTS I would like to thank Stephen Palumbi for his guidance and all of his time, as well as for collecting snails. An additional thank you to the entire Palumbi lab for all of their help and support, and especially for teaching me new lab techniques. And to Peter Marko, thank you for the technical advice and the help with identifying snail shells. -12- Literature Cited Avise, J. 1992. Molecular population structure and the biogeographic history of a regional fauna: a case history with lessons for conservation biology. Oikos 63:62-76. Burton, R., M. Feldman, and J. Curtsinger. Population genetics of Tigriopus californicus (Copepoda: Harpacticoida): I. Population structure along the central California coast. Marine Ecology Progress Series 1:29-39. Burton, R., and M. Feldman. 1981. Population genetics of Tigriopus californicus: II. Differentiation among neighboring populations. Evolution 35(6):1192-1205. Crothers, J. 1984. Some observations on shell shape variation in Pacific Nucella. Biological Journal of the Linnean Society 21(3):259-282. Folmer, O., M. Black, W. Hoeh, R. Lutz, and R. Vrijenhoek. 1994. DNA primers for amplification of mitochondrial cytochrome coxidase subunit I from diverse metazoan invertebrates. Mol. Mar. Biol. Biotechnol. 3:294-299. Gavrilets, S., H. Li, and M. Vose. 2000. Patterns of parapatric speciation. Evolution 54(4):1126- 1134. Hellberg, M. 1994. Relationships between inferred levels of gene flow and geographic distance in a philopatric coral, Balanophyllia elegans. Evolution 48(6):1829-1854. Hellberg, M. 1995. Stepping-stone gene flow in the solitary coral Balanophyllia elegans: equilibrium and nonequilibrium at different spatial scales. Marine Biology 123: 573-581. Kimura, M., and G. Weiss. 1964. The stepping stone model of population structure and the decrease of genetic correlation with distance. Genetics 49:561-576. Marko, P. 1998. Historical allopatry and the biogeography of speciation in the prosobranch snail genus Nucella. Evolution 52(3):757-774. Marko, P., A.R. Palmer, and F. Vermeij. 2003. Resurrection of Nucella ostrina (Gould, 1852), lectotype designation for N. emarginata (Deshayes, 1839), and molecular genetic evidence of Pleistocene speciation. The Veliger 46(1):77-85. McFadden, C., and K. Aydin. 1996. Spatial autocorrelation analysis of small-scale genetic structure in a clonal soft coral with limited larval dispersal. Marine Biology 126:215-224. Palmer, A.R., S. Gayron, and D. Woodruff. 1990. Reproductive, morphological, and genetic evidence for two cryptic species of northeaster Pacific Nucella. The Veliger 33(4):325-338. Palumbi, S. 1992. Marine speciation on a small planet. Trends in Ecology and Evolution 7:114- 118. Palumbi, S. 1994. Genetic divergence, reproductive isolation, and marine speciation. Annual Review of Ecological Systems 25:547-572. Sanford, E., M. Roth, G. Johns, J. Wares, and G. Somero. 2003. Local selection and latitudinal variation in a marine predator-prey interaction. Science 300:1135-1137. West, Lani. Intertidal variation in prey selection by the snail Nucella (=Thais) emarginata. Ecology 67(3):798-809. Wright, S. 1943. Isolation by distance. Genetics 28:1 14-138. -13- Table 1. Number of individual snails sequenced from each location. Haplotypes correspond to the numbers on the phylogenetic tree (Fig. 8). Numbers in parentheses are the number of individuals with each haplotype at a location. Haplotype. Location Number of Individuals HMS Protected 1 (2), 2 (11) 13 HMS Exposed 1 (8), 2 (12), 6 (1) JOE 13 1 (2), 3 (8), 4 (2), 5 (1) SOB 7(7), 8 (1) SLO 9 (5), 10 (2) Table 2. Percentage variation within and between populations. Corresponding Fsr values are shown in parentheses. ’ indicates the value was not calculated. JOE SLO HMS SOB 0.218% HMS 0.194% — (0.303) JOE 0.110% 0.546% 0.056% SOB (0.852) 0.105% SLO Fig. 1. Varying shell morphology in A) N. emarginata and B) N. ostrina. C) Rounded "shoulder" morphotype. D) Angular "shoulder" morphotype. E) Adapical tooth. The tooth is the small bump visible on the apical end of the columella. Fig. 2. Unsuccessful PCR reaction with the primers 1490 and 2198. Lane 1 is a 1-kb ladder, lanes 2-1 8 are individual snails and lanes 19 and 20 are the positive and negative controls, respectively. Note only faint primer dimers are present. Fig. 3. Unsuccessful PCR reaction with the primers COla and COIf. Lane 1 is a 1-kb ladder, lanes 2-16 are individual snails, and lanes 17 and 18 are the positive and negative controls, respectively. DNA templates either did not amplify (lanes 1, 2, and 6) or produced several bands (lanes 3-5 and 7-16). Some product is also visible in the negative control, indicating this reaction was contaminated. Fig. 4. PCR reaction with the primers COIM-H and COIM-L. Lane 1 is a 1-kb ladder and lanes 2-20 are individual snails. Lanes marked with dots represent amplifications good enough for sequencing. Fig. 5. A) PCR reaction with the primers Nucella COIf and Nucella COIr. Lane 1 is a 1-kb ladder, lanes 2-7 are individual snails, and lanes 8 and 9 are the positive and negative controls, respectively. Lanes marked with dots represent amplifications good enough for sequencing. B) Corresponding chromatogram. Note the peaks are all clearly defined and fairly uniform in height. Fig. 6. Haplotypes found at each location. Fig. 7. Location of collection sites and the species found at each location. Fig. 8. A parsimonious phylogenetic tree created from COI sequences. The numbers on the right of the branches correspond to haplotype numbers. Fig. 9. A phylogenetic tree showing branching that occurred in at least 50% of 100 parsimony trees. Numbers indicate the percentage of trees displaying each branching pattern. Fig. 10. Differences in COI haplotype frequencies between wave exposed and wave protected areas at Hopkins Marine Station. Fig. 2. Fig. 3. Fig. 4. Fig. 5. 2 .. B) GC ITTATIGICIGAGC ICATCATATAT TTACAGIGGGAAL L ALTNTRRENW Fig. 6. Monterey Bay HMS - JOE SOB 2 SLO Fig. 7. Monterep be) IIMS — JOE— SOB • N. ostrina • N. emarginata SLO Fig. 8. — 0.1 changes 46510 47S10 48 S10 49 S10 51810 50stc 52 s10 P2HME EAHME -29HNE -30 HNE -31HME E32 HNS E33HNE E3AHNE E35 HME E36 HNE E37HNE Ed3HNE EA4HNE P53 HME P54HNE P55HME P56 HME P5T HNE P58 HNE P59 HME P6O HME P6IHNE P62 HME E56 JOE P75 JOE E9 SOBF EIISOBF E12 SOBF E13 SOB EIASOBF E15 SOBF E16 SOBF PIHNE PSHME ESHME E6 HNEF E3SHE E40HNEF EAIHNE E42HNE E45HNBE E63 JOE E64 JOE E65 JOE E68 JOE E69 JOE MT1 JOE MT3 JOE MTA JOE — NTO E 5 — E17 SOBF 8 MT72 JOE 1P76 JOE -ETHME 6 Fig. 9. 53 53 53 — 100 — PIHNE - P3HME ESHME - E6 HNEF E38 HMEF -E39HMEF -E40 HMF — E41HME -E42HME - E45 HMEF -P2HNE —EAHME -E29HME -E30HME E3IHME -E32 HME -E33HME -E3AHME -E35HME -E36HME -E3THME -Ed3HNE -E44HME P53HME -P54 HME - P55 HME - P56 HME P57 HME — P58 HME - P59 HME P60 HME P6IHME -P62 HME -E63 JOE -E64 JOE -E65 JOE - E66 JOE -E68 JOE -E69 JOE MTO JOE - M2 JOE - P76 JOE -MT1 JOE -MT3 JOE -MTA JOE - P75 JOE -ETHME -E9 SOBF -EIISOBF -E12 SOBF -E13 SOBF -EI4 SOBF -E15 SOBF -E16 SOB -E17 SOBF - 46S10 -47510 -48S10 -49S10 -50stc -52S10 —51st0 Fig. 10. Protected Exposed PPENDIX. Sequences for unique haplotypes found at all four locations, plus previously published haplotypes for N. ostrina and N. emarginata (Marko 1998). 40 20 CTCATATTGTGAGCCATTATTCAGCTAAAAAAGAAACATTTGGAACTT [48 ostrina haplotype 25 emarginata haplotype 19 481 ...........G.................................... [48 haplotype ...........G.o. 481 haplotype ........G..ccccccc. 481 haplotype ..........G..ccc...... haplotype ...........G..ccco [481 haplotype 5 ...........G.................................... [481 haplotype [48 ooooooooooooooooooooooooo. 48 haplotype cccceceoocooooooooooooooosoded. [481 haplotype oecooeooeeeeooeoeoeeeesosoo haplotype9 ..........G.c 481 haplotype10 2223333333.G.................................... 1381 70 80 90 50 60 Sstrina haplotype 35 TAGGTATAATTTATGCAATATTAGCTATTGGGGTTTTAGGTTTTATTG 196 emarginata haplotype 19 196 ........................................C....... ........................................C....... 1961 haplotype 1961 ............cc.ccC.. haplotype haplotype 196 ........................................C....... 196 haplotype ........................................0....... haplotype ........................................C....... [96 1961 ........oooa haplotype haplotype 196 acoooooooeooooeeooooooooooooooooo 196 haplotype 8 .ooooooooooooooooooooooooooooo. haplotype9 ..........coooc. 1961 ..........c. 1861 haplotype 10 ostrina haplotype 25 emarginata haplotype 19 haplotype haplotype. haplotype haplotype 4 haplotype 5 haplotype haplotype" haplotype 8 haplotype 9 haplotype 10 ostrina haplotype 25 emarginata haplotype 19 haplotype 1 haplotype 2 haplotype haplotype 4 haplotype 5 haplotype aplotype haplotype haplotype9 haplotype 10 ostrina haplotype emarginata haplotype 19 haplotype 1 haplotype 2 haplotype3 haplotype 4 haplotype 5 haplotype 6 haplotype haplotype haplotype haplotype 10 110 120 130 140 100 TCTGAGCTCATCATATATTTACAGTGGGAATGGATGTAGATACACGAG 144 eccceoooooooooooeooooo. (144 144 eeooeeeooooeooooooooooooo.. eooooooooeooooooooooooooooooooooo. 1441 1441 oeeeeceeoooooooooooooooooooooooooo (144 ccceeooooooooeoooooooooooooo. (1441 eeoooooooeoooooooooooo (1441 cccccccccccccoooooooooo. ...N....................N....................... (1441 ...N......C.............N....................... 1441 (1441 acooooooooooooooooooooo. aeccccooeoooooooooooooooooooooooo. (134 190 150 160 170 180 CTTATTTTACAGCTGCCACAATAATTATTGCTGTACCTACAGGTATTA (1921 192 ooooeooeoeeeooeoo.. (192 cecccccceceoooooooooooo. 192 aooooeoooeooooooooooooooo. (1921 aoooooooooooooooooo 1921 aooooooooeoooooeeooooooooooooooo (1921 aaooooooooeoooeeoeooeooeoeeoooo. (1921 ooeeeooooooooooeeeooso.. (192 aoooeoeeeoeeeoeooseooeeoooeosoeoe. 1921 ccccc..... (1921 acececeocooooooooooooooooooooooooo. 1821 ........ccccccccG.cc.... 230 200 210 220 240 240 AAGTATTTAGATGATTAGCCACGATTCATGGTGCTAAAATTAAGTATG 240 .ceeoooooooooooooooooooooo. 240 .aaooooooooooooo. 240 ...oooooooooooeooooooooooooo. 240 .aeoooooooooooooooooooooooooo. 240 aaaooooooooooooooooooooooooooooo. 240 acooooooosoooseoeoeoooo. 240 aeoeoeeeoooeeoooooosoeo. .........N.......N.............................. 240 (240 .........N.......N.............................. 240 ..ooooo. 230 .cooeeeoooooeoooooeooooooooo. ostrina haplotype 25 emarginata haplotype 19 haplotype haplotype 2 haplotype haplotype 4 haplotype 5 haplotype 6 haplotype 7 haplotype 8 haplotype 9 haplotype 10 ostrina haplotype 25 emarginata haplotype 19 haplotypel haplotype 2 haplotype 3 haplotype 4 haplotype 5 Saplotype 6 haplotype. haplotype8 haplotype haplotype 10 ostrina haplotype 25 emarginata haplotype 19 haplotypel haplotype haplotype haplotype 4 haplotype 5 haplotype 6 haplotype haplotype 8 haplotype9 haplotype 10 270 250 260 280 AAACACCTATATTATGGGCACTTGGATTTATTTTTTTATTTACAGTAG coccoeoooooooo eoooooo. oooooooeeoooo.. aaoooeoeoeooo ooooooooooooooooooooooooooooooooo eeooeeeeeeeeeeeoeeseeeeeeeeeseeo.. ecaecccooeoeoeeoeooeeoooeoooooooo. aoeoeeoooo. oooooooooseoooo. oooooooooo. aaeocoooooeoeooooooeoooooooeeoooooo. 290 300 330 310 320 GAGGTTTAACAGGGATTGTGTTATCTAATTCTTCTTTAGATATTATGA .....C..............C.........T................. .....C..............C........................... .....C..............C........................... .....C..............C........................... .....C..............C........................... .....C..............C........................... ooooooooooeoesoooooo. ooooooeoooooooooooooooooooooo. eaaaooooooooooooooooooseooooooo. eoooooooeeoeeeeoeeeeoeeeoeeeo. oooooooooooooooooo. 340 370 350 360 380 TGCATGATACTTACTACGTAGTTGCTCATTTTCATTATGTTCTATCAA ...............................C................ eoooooooeooeoooeoooooooseooooo. aooooeooooooeoeooeooeeooooo eooooooooooooooooooo. ........................................C....... .........ccccccccC...... .............T.................................G. .c.oooooooo. ccceoooo. oooooooeooooooo eeoeceeeeoeeeeeeeeeeoeeeoeseeoeo. (288 288 (288 288 2881 2881 288 288 288 288 288 (2781 [336 (336 (336 [336 [336 (3361 (336 [336 3361 336 [3361 [326 384 [3841 (384 [3841 (384 [3841 (384 3841 3841 (3841 [384 (3741 ostrina haplotype 25 emarginata haplotype 19 haplotype 1 haplotype haplotype haplotype haplotype 5 haplotype haplotype 7 haplotype 8 haplotype 9 haplotype 10 ostrina haplotype 25 emarginata haplotype 19 haplotypel haplotype haplotype3 haplotype haplotype aplotype haplotype haplotype haplotype haplotype 10 390 400 410 420 430 TAGGAGCAGTTTTTGCATTATTTGGAGCTTTTAATTATTGATTTCCTC ...G....ccccccccccccccccccccccecc ....G.....ccc.. ....G....ccccc......... ....G....cc..... ....G....ccccc.. ....G....ccccccccccccc oooooooooosooooooo eeeesoeeeeeceoseeseeeeeeeeeeeeeoeoosee.. eoooooeeooooeeooeeseeeesooo eaaooooooooo ooooooooo.. 480 440 450 460 470 TTTTAAGGGGTGTTTCGCTTCATAGTCGTTGAACTAAAGCCCATTTTT aoooooooooooooooooooooooooooooooo . . . . . . . . . . . . . . . . . . ...............22 .... ...............C............. ...................C............. ........................... .....GAG.::::::::::: .......T........ .. .....T............. .......T............ .. . . . . . . . . . . . . . . . . . . . . ..........22 ................................. (4321 (4321 [4321 (4321 [4321 432 4321 4321 [4321 432 432 (4221 [480 480 [4511 4631 (4641 [463 468 [451 (4511 4511 463 [4531