INTRONUCTTON Pt. Pinos is located in Pacific Grove at the southern end of Monterey Bay. A large portion of the point is a rocky intertidal region. The rock-filled tide pools and abundant algal growth provides an ideal area for the starfish Patiria miniata, (Brandt, 1835) to grow. However inthe immediate vicinity of the Pacific Grove sewage outfall the intertidal region has been seriously disturbed, and there are no Patiria living there. My project was designed to determine whether the paucity of Patiria could be attributed in part to the effects the sewage might have on either the adults, the gametes, or the early developmental processes. I found that, in the highly polluted areas near the outfall, the sewage killed the adults and in lower con- centrations inhibited their feeding processes. In addition chlorinated Pacific Grove sewage reduced the success in fertilization with full fertilization only being achieved below a 0.1% dilution. Even very low concentrations of sewage were strong enough to cause a decrease in the rate of development in the embryos. Hypochlorite, the only individual component of the sewage which was tested for toxicity, appeared to be the major toxic constituent. It caused a reduction in the fertility of the eggs and a decrease in the ability of the sperm to effect fertilization. METHODS AND MATERIALS For each experiment gametes were taken from a single male and a single female. The web between two rays was cut to the central disc, and the gonads removed with tweezers. To prepare the ovaries, they were washed twice with filtered sea water and placed in 25 ml of sea water in a beaker. Two ml of 10 M 1-methyladanine was then added to the eggs to stimulate shedding and meiosis (Stevens, 1970). One to two hours were necessary to complete the shedding process. The eggs were then divided into separate aliquots for the various experiments. A testes, removed from a male 5 to 10 minutes before fertilization, was washed once with filtered sea water and then placed in 50 ml of filtered sea water. Four-tenths ml of this solution was used for fertilization of each aliquot of eggs. Since fertilization success is related to the sperm concen- tration, this standard volume provided a large excess of sperm, while it kept the amount of sperm added to each sample constant within any one experiment. Using a standard also minimized the variation between expeniments. One hundred and fifty to two hundred eggs were counted to yield the percentages for the recorded data. The series of sewage dilutions that were used in the experiments was 100, 50, 10, 5, 1, 0.5, and 0.1% by volume. Filtered sea water was used to prepare these dilutions, and the solution was made isotonic by the addition of sea salts. In the experiments using hypochlorite, a stock solu- tion of 40 ppm was prepared using filtered sea water and reagent grade Naocl. To terminate the exposure of eggs to hypochlorite, the solution was drawn off and the eggs washed twice with filtered sea water. Rather than wash sperm to conclude their exposure to hypochlorite, an excess of Na,S,O, was added to neutralize the hypochlorite. The temperature was maintained between 12° and 15 9c by placing the test vessels in a plastic tub on the sea table. RESULTS Population Survey A rough study was made of the Patiria population on Pt. Pinos. The intertidal region was examined at low tide on three successive days and the general location and number of any Patiria found was noted on a map. The study may not reflect the natural distribution because of the difficulty in locating all of the animals, and also because the point is accessible to the public and animals may have been removed or transfered. There were no Patiria found on the south side of the point from the channel west of the outfall all of the way through Cove C. Three adults placed in a cage in area A about 15 meters from the outfall were killed within 24 hours. The starfish living closest to the outfall was found on the edge of a highly damaged area at the mouth of Tide Pool wl. There were a few individuals found in the rocks mainly on the seaward side of that tide pool where they were getting fresh sea water during most of the day. The population density continued to increase toward the western end of the point. On the northern side there was an even distribution all of the way down the point. Feeding Behavior To test the effect of sewage on feeding behavior Patiria were starved for two weeks by keeping them in a tank without food. They were then placed into dilutions of both chlorinated and unchlorinated sewage and 16 hours later a fresh Mytilus californianus was cracked open and placed under each animal. In a 5% concentration of sewage Patiria were less apt to eat than when they were in fresh sea water. When the concentration was increased to 10% they did not eat at all. The starfish kept in sewage were then placed back in fresh sea water. After 5 hours they were again given a mussel, and all of them began to eat within 5 minutes. Embryonic Development in Pt. Pinos Water Current studies of Pt. Pinos, done by students of Hopkins Marine Station during April, 1970, indicate that the sewage leaving the outfall was carried toward stations 1, 2, and 3. Fertilization was drastically affected in water samples taken from this area (fig. 1). However once the egg was fertilized, except in water from station 3 more than 94% of the eggs were able to reach the blastula 16. stage. No bipinnaria larvae were later found in the samples raised in water taken from stations 1, 2, or 3 and the larvae raised in waten taken from stations 4, 5, and 6 were indistinguishable from the control. Fertilization The process of fertilization is affected by sewage (fig. 2). Full fertilization is not attained until there is a substantial dilution of the sewage. If it is chlorinated, fertilization is affected over an even greater range of dilutions (fig. 2). When fertilized and allowed to develop for an hour before being placed into sewage, the eggs were still sen- sitive to sewage more concentrated than 5% (fig. 3). In 100% Monterey sewage, most of the eggs reached the 8- to 16-cell stage before stopping. Eggs placed in the unchlorinated Pacific Grove sewage only attained the 4- to 8-cell stage gefore being arrested. None of the eggs in the chlorinated Pacific Grove sewage got beyond 1 cell, and most of them were cytolyzed and had lost all internal unity (plates 1,2). Because of the differences shown between the chlor- inated and unchlorinated Pacific Grove sewage, further work was done on the effects of hypochlorite (the major product of chlorination, see Imhoff and Maskew, 1956). In sea water containing 40 ppm hypochlorite, the tails of the sperm became twisted and often broke. As the solutions became more dilute, physical effects were not as 16 apparent; however no fertilization was achieved with sperm that had been exposed to concentrations of hypochlorite greater than 0.4 ppm. In contrast to the effects of hypochlorite, no morphological effects of unchlorinated sewage were observed with sperm or eggs. The eggs are not as sensitive to the hypochlorite as the sperm. After being exposed for 45 minutes to a 40 ppm solution there is no fertility, but full fertili- zation is achieved by eggs when they are exposed to a 4.0 ppm concentration of the hypochlorite, washed, and then fertilized. The above results suggest that hypochlorite is the major toxic ingredient in chlorinated sewage. To test this, a hypochlorite solution in sea water was prepared which was equivalent to the 'available chlorine' content of a sample of chlorinated sewage. Eggs were then fer- tilized in various dilutions of these two solutions. The results, seen in figures 4 and 5, show that the effects on both fertilization and development were very similar, with the hypochlorite solution being only slightly less toxic. DISCUSSION The gametes, early developmental stages, and adult Patiria are all affected by sewage and its associated levels of chlorination. Through its gametes, the starfish is sensitive to concentrations of hypochlorite higher than 66 0.2 ppm. Effects on the adult ranged from an abstinence from feeding behavior in concentrations greater than 5% sewage to death within 24 hours when placed near the outfall. The most probable reason the animals did not eat in highly polluted water is that Patiria locates food by chemoreception (Hyman, 1955). In high concentrations of sewage the sensors might not be able to recognize or detect the presence of food. Monterey sewage, which was unchlor- inated, did not inhibit the feeding behavior below a concentration of 10% sewage. In contrast Pacific Grove sewage affected the feeding behavior at dilutions of 5%; perhaps the hypochlorite has an effect on chemoreception, also. The results showed that the fertilization process was highly susceptible to sewage and hypochlorite. Thus, more than twice as many embryos were able to reach the blastula stage in 10% and 5% sewage dilutions if the eggs were fertilized before they were placed in the solutions. That not all embryos in 5% to 10% sewage dilutions successfully reached the blastula stage suggests that there are other toxins in the sewage, which interfere with processes of division or blastulation. Alternatively the same toxins may be present, but the embryo may be partially isolated from the environment by the presence of the fertilization membrane. The comparison of chlorinated versus unchlorinated sewage showed that chlorinated sewage was far more toxic 16. to development. As shown, the active agent in chlorinated sewage was hypochlorite, and the sperm were more sensitive than the eggs. The sperm were sensitive to hypochlorite concentrations as low as 0.2 ppm, whereas eggs could be fertilized after an exposure to 4 ppm. Thus the sperm was the critical gamete in regards to chlorinated sewage. The experiment comparing chlorinated sewage to a sea water solution containing the same amount of 'avail- able chlorine' in the form of hypochlorite, yielded the surprising result that the pure hypochlorite solution was almost as toxic as the chlorinated sewage. The effects of the hypochlorite simply over-rode most of the effects of the sewage rather than being additive. This is some- thing that should be more thoroughly investigated since light, agitation, and organic constituents can cause a breakdown in hypochlorite, and an increased rate of hypochlorite decomposition in the sewage solution might have made the two solutions appear more similar than they really were. It is surprising that the oxidized and chlorinated organics resulting from the chlorination did not present a greater barrier to fertilization and development. These results are not conclusive enough to esplain the observed distribution of adult Patiria on Pt. Pinos. However they do indicate that the region on the south side of the point from the channel west of the outfall eastward through Cove C is unsuitable as a breeding site for Patiria. Most importantly, the present results show that fertilization is sensitive to very low levels of hypochlorite. Therefore, down current from the outfall in areas where the sewage has been so diluted as to produce no obvious damage and to be hard to detect, it may still present a significant ecological threat. SUMMARY The gametes, early stages of development, and adult Patiria are all affected by sewage and its asso- ciated levels of chlorination. Effects on the adult ranged from an abstinence from feeding behavior in concentrations of sewage greater than 5%, to death within 24 hours when placed near the outfall. The fertilization process was somewhat sensitive to unchlorinated sewage and highly sensitive to chlorinated sewage. Thus, more than twice as many embryos were able to reach the blastula stage in 10% and 5% sewage solutions if the eggs were fertilized before being placed in the sewage dilutions. Hypochlorite was found to be the active ingredient in chlorinated sewage. The sperm were more sensitive to the hypochlorite than the eggs, showing a reduction in the ability to fertilize eggs in concentrations as low as 0.2 ppm. Because of the high sensitivity of fertilization to both chlorinated and unchlorinated sewage, the ecological effects of the sewage may extend far down current from the damaged area near the outfall. 16 C C S Toesdo 4 TIDEPOOL 2. 3 OUTFAL 28 V /6. 100 80 60 40 20 a alb alb alb 4 a alb 16 5 —- O 71 bab 17 81 —— S 17. 54 S oh 17 200x 14 aee at 15 ae.ded. oseded. 7 EIGURE LEGEND Abscissa: station number; ordinates: percent response. Fig. 1. Eggs fertilized and raised in water taken from stations at Pt. Pinos. a: percent fertilized; b, percent of the fertilized eggs that reach the blastula stage in 14 hours. Figs 2-5. Uchlorinated Pacific Grove sewage, OC unchlorinated Pacific Grove sewage, AA Monterey sewage, kAsea water with hypochlorite added. Abscissa: percent sewage concentration; ordinates; percent fertilized. Fig. 2. comparative graphs for fertilization in sewage dilutions. Chlorinated Pacific Grove sewage had 37.4 ppm hypochlorite. Abscissa: percent sewage concentration: ordinates; percent of the eggs fertilized that reached blastula stage in 22 hours. Fig. 3. comparative curves for development in sewage dilutions. Chlorinated Pacific Grove sewage had 37.4 ppm hypochlorite. Abscissa: percent sewage or hypochlorite by volume; ordinates: percent fertilized. Fig. 4. comparative curves for fertilization in chlorinated Pacific Grove sewage and sea water with hypochlorite. The undiluted solutions both had 14.9 ppm hypochlorite. Abscissa: percent sewage or hypochlorite by volume; ordinates: percent of the fertilized eggs that reach the blastula stage in 12 hours. Eig. 5. comparative curves for development in chlorinated Pacific Grove sewage versus sea water with hypochlorite. The undiluted solutions both had 14.9 ppm hypochlorite. Fig. 6. a normal fertilized Patiria egg. The fertili- zation membrane and polar bodies may be seen. Eig. 7. a cytolyzed Patiria egg after exposure to a 20 ppm hypochlorite solution. ACKNONLEDGENENTS am especially indebted to Dr. David Epel for the encouragement and assistance he gave me on my project. I should also like to thank the faculty and staff of Hopkins Marine Ststion for making this quarter the valuable experience that it was. RERERENCES 1. Hyman, L H, The Invertebrates, McGraw-Hill Book Company, New York (1955) Vol IV, 273. 2. Imhoff, K and Gordon M Fair, Sewage Treatment. John Wiley and Sons, Inc., New York (1940) 162-171. 3. Stevens, P, Explt cell res 59 (1970) 482-485.