Abotract Different methods of inducing spawning in the gastropod Achea incessa were investigated. No reliable method was found that could be used as a generalized technique for mollusc spawning. To stain the chromosomes of the eggs and developing zygotes, used a method that required preliminary fixation in carnoys solution followed by DAPI stain. The developing stages of the zygote chromosomes immediately l17 after fertinzation up until the first cleavage are documented. Introduction Oogenesis, fertilization, and development of the embryo has been studied extensively in echinoids (Strathmann, 1987 ). Part of sse gametes have been used is the ease with which they theresonth can be studied There are standard methode for constanthy inducing spawning and large amounts of gametes can be obtained. Also, the eggs are transparent enough to get a clear view of the internal ages of developr organization of the egg during the first ent Molluscan egas have been studied little in the past because working with the animaje and the eggs ie difficult. There are no phabeme hods for inducing spawning. Also, the egge are coaqde and d n inquishable theic + norder to learn more about spawn zyocte development in molluscs,have used th haveteted various epawning techniquee and aleo egaed differenth for omosome aining proceud i obtained directions from Dr. Daniel Mazia and Dr. Linda Goff. With the tools for chromosome staining, have determined the nuclear cytology of eggs and the early stages of developing zygotes. Materials and Methods Handling of gametes: Acmea incessa were collected at the shorline in Pacific Grove and Carmel California and kept on fronds of Egregia menziesi in an outdoor running sea water tank. The tank was covered with a screen mesh which diffused the bright afternoon sun but allowed enougn illumination to keep the Egregia in good condition without allowing the water in the tank to become too warm. In compliance with Sharon Proctor 's thesis (1968), to induce spawning of the animals, six to nine individuals were removed form the tank and placed in separate glass dishes filled with fresh sea water that subsequently was allowed to slowly reach room temperature (between 18eand 22 0. As soon as a female animal spawned, the eggs were removed with a Pasteur pipet and placed in filtered sea water (FSW) in a 16C cool room. Spawned eperm was similarly removed but placed immediately into a6Ccold refridgerator. To induce increased gamete release fter an animal had apawned, some streams of water were auned at the foot or the dish was jiggled. Eggs were fertilized within one and a half to two hour wring by adding a few drope of dilut sperm to the egg-row mixture. Sperm stored for up to two days at 6 C could still be used for fertilization. In sgme cases, eggo were aloo acquired by disecting females in ammonia sea water (sea water titrated to pH 9.5 with MOH). The ammonia sea water causes gernimal vesicle (GV) breakdown. while holding the animal in the ammonia sea water, an incision was made in the gonad and oocytes flushed out of the opening. The released oocytes were allowed to settle to the bottom of the dish and the excess sea water was removed by aspiration. The eggs were then placed in fresh ammonia FSW and allowed to sit for one to two hour until GV breakdown which is necessary before normal fertilization çan occur. After GV breakdown and before fertilizing, the eggs were transferred to normal sea water. Fixing and staining techniques: Eggs suspended in FSW were centrifuged, the sea water aoys fixative remoyed by aspiration, and the eggs resuspended in Carii (Jethapol; 1 acetic acid). After and hour of fixing in carnoys, the eggs were washed in a 707 ethanol solution and recentrifuged. The banol was removed by aspiration and the remaining ces were allowed to evaporate. The eggs were resuspended in FSW and 4,6-diamidino-2-phenylindole (DAPD) stain was added to make a final concentration of Sugimi (Linda Goff, 1962)DAPI (Sigma Corporation / wes in astock solution of 1ma/mi in dimethylsulfoxidet OMSO). After fifteen minutes of staining, the eggs were viewed under a fluoreceence mierescepe witha UV filter to determine the cytological state of the chromosomes. To examine fertilized eggs by the DAPI procedure thee ronase (Sigma Corporanon) before fixation we ted wit remoye excess sperm. Sixty ml of pronase stock (Img/mi) was added to every Iml quantity of egg-FSW solution. Usually pronase stock was added to egg-FSW mixture four minutes after insemination (in one case at two minutes). The fertilized eggs were suspended in propase-FSW mixture for one to two minutes and gently shaken. The fertilized eggs were then washed twice with FSW to discard the pronase. Other fixing and staining techniques Carpoys was also used without DAPI. Eggs suspended in F5w were centrifuged and the FSW removed by aspiration. The eggs were resuspended in carnoys solution for one hour before being washed with 458 acetic acid. The eggs were viewed under a phase microscope. Adetergent-extacted-DAPl prdocedure was also Used to visualize the chromosomes of the egg (Dr. Daniel Mazia). Eggs were centrifuged in ESW and the pellet resuspended in KGE solution of ph 6.8 (29 potassium gluconate, 306M glycine, 2mM potassium ethylene glycol bis-(B-aminoethylether) N,N,N,N-tetraacetic acid,VEGIA MA MaSO Stock solution of EGTA is dissolved by titrating with For to about pH 6.5). The eggs were centrifuged again and restien suspended in detergent-DAPI soluticn (made with ten volumes of FGE-pH58 and one volume 103 Triton X-100). Then DAPI was added to make a final concentration of lugml The staineg ec reviewed fuorescent microscope. Reoulto Spawning: Spawning induced by placing individuals in warm sea water was incopsistent. Often times no spawning would occur at all while at other times, every individual in the dishes would spawn. My impressions of the phenomina were that Acmea incessa released gametes more often if the animals were used on the same day of collection than if they had been stored in the outdoor tank for a few days before being used. Disection: The limpets that did not spawn were saved for disection. 10 distinquish between male and female gonads, the animal was cut out of it'sshell. On the dorsal surface, aside the visceral mass, the gonad was visible. The male gonad appeared orange with smalk creamy white dots. The femal gonad appeared brown. The disected female gonads provided eggs with intact GVs. he GV broke down after an egg sat in ammonia FSW pH9.S for one to twe hours. Out of four separate attempts at fertilizing disected eggs, only one attempt was successful. The disected male gonads provided mostly nonmotile eperm. A few procedures were tried in order to induce motility. Asmall drop of EDEA PH 8.0, a crystal of cysteine, and a small drop of spawned sperm supernatant were all separately added to large drops of disected sperm on microslides and viewed under a dark field microscope. All of these procedures produced negative resulte. One more method of spawning induction was tried. Ten mM gamma amino butyric acid (GABA) was injected into the foot. The response was foot flexion and inability to grip the glass dish. No spawning occured. Light microcope observations: Spawned unfertilized eggs appeared opaque and orange-brown under the phase microscope. No GV was present and internal structures were not easily visible. A jelly coat surrounded the eggs but was not apparent unt il sperm was added. The coat was made apparent by the clear separation between the surrounding sperm and the egg surface. Eggs obtained by disection had a jelly coat but also had a GV that was seen with dark-field. With this illumination, the GV was seen as a white-orange circle inside the darkere colored egg. Äfter GV breakdown, the eggs obtained by disection appeared identical to spawned eggs. Fixation and staining techniques: The carnoys-DAPI staining technique provided the best ar behavior. The chrome visualization of chromosomes and nucle and sperm DNA were seen in great detail as fluorescent blue t uctures under the fluorescent microscope. Chromosome? waseesiettoeithe sarpeofeg ore had acover p and the egas were flattened by pressing againet a paper towe Carnoys alone (no DAPI or other dyes) did not make the chromosomes as visible as the carnoys -DAPI technique. Carnoye fixed the egg and the chromosomes appeared black under phase microscopic illuminations. However, the yolk granules and other cellular structures also appeared black, resulting in difficulty in finding the chromosomes. The detergent-DAPI procedure stained the chromosome similarily to the carnoys-DAPI procedure. However, the fine structure of the chromosomes was not as apparent, appearing as plurred fluorescent dots. Nuclear events. The carnoys-DAPl technique was used to visualize the egg and sperm chromosome structure before and af ter fertilization. Portions of pewly fertilized eggs were fixed with carnoys every five minutes up to the first cleavage. Unfertilized eggs were found to be in rested metaphase IFigure 1). They had not yet gone through the mejotic divisions that produce poiar bodies. Within five minutes after perm addition, cells had bare ly begun to enter anaphase (Figure 2). Between five and fifteen minutes after fertilization, the zygote had formed one polar body (PB) which stayed intact at the edge of the zygote (Figures Jand 4). At twenty five minutes, the meiotic apararus of anaphase Il occured next to the site where the firet PE asformed (Figure 5). Between twenty-five and thirty-five minutes after fertilization, the second PB had formed and remained at the outer edge of the zygote next to the first PE (Eigure eE minutes after fertilization, the zygote was already dividing (Figure 7) The mitotic events must have been rapid, as they were missed. sed DNA was visible as tear-shaped, lobes on each side 04 Deconder the dividing zygote (Figure 7). The two PB's were still attached to the egg and were almost always located at the site of cleavage (Figures 7 and 8). Discussion Acmea incessaindividuals proved to be a difficult species with which to work because all attempts to induce spawning wer upreliable, Disection provided large quantities of gametes, but they were usually not usable. The sperm was always nonmotile and the eggs did not ferilize successfully. There was really no good method of obtaining gametes. With the gametes that were obtained, however, the chromosomes were successfully fixed and stained with the carnoys-DAPI preparation. Using this staining method,was able to account for the cytological changes in the zygote chromosomes up to the first cleavage. As already mentioned, there was a correlation between spawning frequency and the day of collection. It is my impression that the animals kept in the tank spawned there and resultant ly did not have any more ripe gametes ready for release when later subjected to spawning induction methods. This hypothesis is fürther tthe disected gametes from individuals t upported by the fa whpaturally were not functional (except one ce would not sp —heresome dicetedegeeid ferilze). at some hormone other than GAEA may activate tispiet t jon procees. y gsor speed up the matt theeg for Acmea incessa spert Since there is no known method of inducing spawning reliably, suggest that the best way of obtatning functional gametes is to induce spawning by letting the animals sit in warm sea water on the same day that the animals are collected. Also, the water that they are transported in from the intertidal zone should not be allowed to become warmer than 16'C. Spawned eggs were opaque orange and contained no GV contrary t to findings by Sharon Proctor (1968). The eggs had a jelly coat diat was shed after fertilization. Eggs obtained by disection clearly had a GV before spending one to two hours in ammonia sea water at pH 9.5. The eggs also had a jelly coat and not a thick chorion as Sharon Proctor reported (1968). Nuclear evente Carpoys-DAPI was the most lucrative method of fixing and staining Acmea incessa eggs and zygotes. Using this method, the events of egg maturation after sperm entry were visualized cleary. Unfertilized eggs were in arrested metaphase as reported by wilson ( 1919). After insemination, I found that two polar bodies were formed efore the nuclear fusion of the sperm and egg. However, did not fix any eggs at the correct time to capture the mitot t ore detailedaccount ofthenucleare btan a T00 e zygotes could be fixed at narrower time inter fertilization th thanfive minuteshecarnoys-DADtechnige eeprege reliable method for future cytological studies on damea incessa. ed staining my could be a lucrative study using th Poly jethod. However, without a more reljable methe d for obtaining gametes, do not recommend using Acmea incessa as a research subject. References Dube.F., Dufresne-Dube,L., and Guerrier, P.C1982). Sperm Nuclear Decondenstion in Barnia candida (Mollusca, Pelecypoda) Oocytes does not require germinal vesicle breakdown. JExp. Zoology 9 :383-387. 2 Goff.L., (1988). Carnoys-DAPl staining. Personal reference. Hipkley, R.E., wright, B.D., and Lynn, J.W.(1986). Rapid visual detection of sperm-egg fusion using the DNA-specific 77 fluorochrome Hoechst 55942. Devel. Bio. 118,148-154. Kanatani,H. (1985), Oocyte growth. Oocyte maturation. Biology or 0 Fertil tion vol.1,225-240. Mazia.D. (1988). Detergent-extraction-DAPI staining methods. Personal reference Proctor.S. (1968). Studies on the stenotopic marine limpet Aced incessa (Mollusca, Gastropoda, Prosobranchia) and it's host Egregla menziesil (Phaeophyta) Thesis. per oment of ann (1987). Beproduction and Develof a Strathm rthern Pacific Coast. ofthe invertebra ent Wilson,E. (1919). Ihe Cell in Developinenand in Figure Legendo Figures: 1. Lwo upfertilized eggs with the chromosomes visibly in metaphase. 2. Five minutes post-insemination, the sperm nucleus is seen as the smaller dot. The egg nucleus is just beginning to enter anaphase !. 3. Ten minutes post-insemination, the egg nucleus has already funly entered anaphase 1 of mejosis to form the first polar body. 4. Fifteen minutes post-insemination, the eggs nucleus has a formed polar body. S. Twenty-five minutes post-insemination, the egg nucleus is seen in apaphase Il of meiosis. The chromosomes divide next to the site of the first meiotic cleavage. The smaller spot is the sperm nucleus. 6. Thirty-five minutes after insemination, two polar bodies are seen. Sixty minutes after fertilization, mitosis is already complete as can be seen here where two lobes of decondensed DNA have recently separated The third spot is the combination of two polar bodies out of focus. 9. Seventy minutes post-insemination, cleavage is finished and the two polar bodies are seen at the site of the cleavage. Figure 1 Figure 2. 12 Figure 3 Figure 13 Figare 5 Figure . 14 Figare Figure 8. 15