Egg Capsule Sheath Bacteria - 2 ABSTRACT The egg capsule sheath of the squid Loligo opalescens is an acellular matrix 1-2 mm thick which contains roughly 100 thin striations in layers parallel to the capsule surface. In this matrix is suspended a dense culture of bacteria in one to five layers. Its probable source is the accessory nidamental gland. Egg Capsule Sheath Bacteria - 3 INTRODUCTION After mating, female Loligo opalescens deliver their eggs in clusters of 100 to 300, covering them in a sheath secreted by their nidamental glands (Arnold,'71). An ovulating female then attaches this egg capsule, (Fig. 1), to a large, common egg-mass built up by several females on sandy substrate (Recksiek and Frey 78). Local divers report little attrition of these egg masses, and it appears the embryos escape animal, fungal, and microbial predation during their three to five week incubation. An interesting predation defense mechanism or mechanisms may exist. while assessing microbial settlement on the egg capsule surface in a search for this mechanism, we noticed bodies that appeared to be bacteria far below the capsule's colonized surface. We have investigated these bodies and here report the first instance of an apparently natural deposition/colonization of bacteria in the sheath of Loligo opalescens egg capsules. We describe the morphology of the egg-capsule sheath, and detail the distribution of its bacterial flora with electron and light microscopy. Egg Capsule Sheath Bacteria - 4 MATERIALS AND METHODS General: Squid were captured in Monterey Bay, held in 2000 liter, circular holding tanks with constant flow, and induced to mate by artificial egg masses (Yang, '83) Electron Microscopy: After opening freshly laid (age «6 hrs) capsules longitudinally and removing the chorions and embryos with sterile forceps (Fig. 1), samples of the capsule-sheath were fixed in glutaraldehyde (22 in sterile sea water for 2 hrs), treated with osmium tetroxide (12 in sterile water adjusted to oceanic salinity and pH), stained with uranyl-acetate (1 hr at 12, as for osmium tetroxide), serially dehydrated in acetone (20- 1002 in 102 steps), then set in Spurr's plastic (Spurr '69). This block was then sectioned to 800 Angstroms in planes perpendicular to the surface of the capsule, and examined on a Phillips 201 electron microscope at 80 ky. Light Microscopy: The transmission EM protocol described above was followed until the sample had been set in Spurr's plastic. The sample was then sectioned to 3 microns in planes perpendicular to the surface of the capsule, stained with Lee's methylene-blue basic-fuchsin, and examined at 1000x total magnification under oil. Bacterial Distribution: The capsule sheath was separated from the embryos and chorions (Fig. 1), then sectioned in 0.5 mm planes perpendicular to the surface of the capsule. To minimize extraneous bacteria all implements and surfaces in contact with the capsule were sterilized for 10 minutes with 952 ethanol, Samples were then stained with acridine orange (1 ug/ml: 10 minutes stain, 10 minutes wash in sterile sea water) or the DNA specific stain DAPI (4', 6-diamidino-2-phenyl-indole diluted 1 to 1000 in sterile sea water, 20 min stain, 20 min wash in sterile sea water), and examined at 1000x total magnification with UV excitation. By photographing adjacent microscope fields while traversing samples, photo-montages which transected the depth of the capsule-sheath were prepared. Egg Capsule Sheath Bacteria - 5 RESULTS Sheath Structure The sheath is a tough, acellular matrix one to two millimeters thick which completely encapsulates the eggs (Fig, In light and electron microscopy its most obvious structural features are numerous, thin striations parallel to the capsule surface (Fig. 2). These striations, which stain darkly with Lee's-methylene-blue-basic-fuchsin in light microscopy, are also stained by uranyl-acetate in samples prepared for transmission electron microscopy. Both results suggest that these are areas high in protein content. The striations are roughly 3 microns thick, 10 to 20 microns apart. We estimate that the sheath, at 1000 to 2000 microns thickness, contains roughly 100 of these striated layers. Sheath Bacteria In addition to striations, light microscopy also reveals bacteria-sized bodies deep within the capsule sheath (Fig, 2). Transmission electron microscopy further reveals morphologies which strongly suggest bacteria (Figs. 3, 4). Fluorescence microscopy of samples stained with the DNA-specific dye DAPI confirms that these bodies contain genetic material and are therefore most likely bacteria (Fig. 5b). In electron and light microscopy a fusiform bacteria is consistently in high abundance, even in capsules less than six hours old. It stains positively with acridine orange and DAPI, and is present in the sheath of all the capsules we have examined to date (Figs. 4, 5b). The distribution of bacteria through the depth of the capsule sheath, as assessed by optical sections stained fluorescently for DNA, appears to be non-random. One to five densely populated layers, in which bacteria may comprise as much as ten percent of the volume of the sheath matrix, alternate with layers which are nearly or completely free of bacteria. Egg Capsule Sheath Bacteria - 6 By photographing adjacent microscope fields while traversing a section cut through the depth of the sheath, a montage of the bacterial distribution was prepared (Fig. 5a). A composite drawing representing a square centimeter of capsule-sheath viewed edge on, synthesizes the striations visible in direct light with the layered bacterial distribution apparent in fluorescence (Fig. 6). Egg Capsule Sheath Bacteria - 7 DISCUSSION Our observations indicate that the one to two millimeter thickness of the egg capsule sheath contains roughly 100 striations, probably proteinaceous, and one to five densely populated layers of bacteria. Bacteria in organized layers abundant even in capsules less than six hours old, raise questions of origin, function, and generality. Origin If work on Loligo pealei, an Atlantic squid, can be generalized to the Pacific Loligo opalescens, a likely source for the sheath bacteria is the female squid's accessory nidamental gland. In many species of cuttlefish and squid this paired organ of sexually mature females opens onto the mantle cavity, which serves the organism as an oviduct (Williams '09), (Buchner '65). Studies of L. pealei by Bloodgood ('77) reveal that the accessory nidamental gland derives its mottled appearance from internal convoluted tubules, which harbor one of three distinct cultures of bacteria (one of which produces a sepiaxanthin-like pigment responsible for the gland's color). Bloodgood's investigations further show the gland has musculature permitting it peristaltic movement and is contractile upon dissection from the squid. His results also suggest that the gland secretes a medium on which the bacteria grow. while the capsule sheath is secreted primarily by the nidamental glands, (Arnold '71), the duct opening of the accessory nidamental gland suggests that it may also contribute to formation of the capsule. Our results suggest that its contribution could include bacteria. Perhaps the accessory nidamental gland contracts during formation of the egg capsule, periodically expressing its bacterial contents into the sheath, This would account not only for the layered distribution, but also for the abundance of bacteria in newly laid capsules. Egg Capsule Sheath Bacteria - 8 This phenomenon is not unprecedented. Early investigators of bacteria in the accessory nidamental glands of bioluminescent squid (Pierantoni '14, '18), (Herfurth '36), (as cited in Buchner 65) noted bacteria in the egg capsule sheaths of three squid: Loligo edulis, Loligo forbesi, and Sepia officinalis. These investigators also looked on the accessory nidamental gland as the most likely source for the sheath bacteria, Function Function of egg capsule sheath bacteria is perhaps the most interesting question raised by this study. A likely pezibliig is defense of the developing embryos. Loligo opalescens' eggs are laid in large masses which appear to suffer little animal, fungal, or microbial attrition. Sheath bacteria offer a possible explanation for this predation resistance. Instances of natural flora discouraging colonization by pathogenic organisms have long been established (Zobell '46). Sheath bacteria might populate layers of the capsule sheath so heavily that all available resources are exhausted to the detriment of pathogenic organisms. It is also possible that the bacteria do not "passively compete" but actively produce an antibiotic compound. A symbiosis of this type has been noted in a crustacean's eggs, in which a bacteria of the genus Alteromonas protects embryos by producing the fungicide isatin (Fisher '83, Gil-Turnes, Hay, and Fenical '89). If "embryo protection" is actually a role of sheath bacteria, it may not be the only element in the capsule with this function. Atkinson ('68, '73) has demonstrated an "immobilizing factor" in the nidamental gland secretions which form the capsule sheath. This factor agglutinates the cilia of motile metazoans, and may inhibit protozoan predators of the egg capsule. Sheath bacteria, in conjunction with "immobilizing factor" might constitute an interesting system of embryonic defense. Egg Capsule Sheath Bacteria - 9 Generality Already noted in the egg capsule sheaths of three bioluminescent squid (Buchner '65), and now a non-bioluminescent squid (Biggs and Epel '90), egg capsule sheath bacteria may be a more general phenomenon than previously suspected. Marine bacteria have also been found in association with the eggs of a scaphapod (Geilenkirchen, Timmermans, Van Dongen, and Arnolds, 70), and even a crustacean (Fisher, '83). In the cephalopods investigated so far, it appears sheath bacteria are derived from the accessory nidamental gland. Since this organ is common in squid and cuttlefish, it is conceivable that further investigation will reveal other instances of accessory nidamental gland-derived sheath bacteria. If so, the function of accessory nidamental gland bacteria, which has remained elusive in adults (Bloodgood '77), might become evident in the context of the capsule sheath. LITERATURE CITED Atkinson, B., and N. Granholm (1968). A ciliary activity inhibitor extracted from the nidamental gland of Loligo pealei. Biol. Bull., 135: 413. Atkinson, B. (1973). Squid nidamental gland extract: isolation of a factor inhibiting ciliary activity. J. Exp. Zool, 184: 335-340 Arnold, J. (1971). Cephalopods. In: Experimental Embryology of Marine and Fresh-water Invertebrates. G. Reverberi, ed. North Holland, pp. 265-311 Biggs, J., and Epel, D. The egg capsule sheath of Loligo opalescens: structure and association with bacteria. J. Exp. Zoo. Bloodgood, R. (1977). The squid accessory nidamental gland: ultrastructure and association with bacteria. Tissue and Cell, 9(2): 197-208. Buchner, P. (1965). Endosymbiosis of Animals with Plant Microorganisms. Interscience, New York, pp. 543-571. Fisher, W. (1983). Eggs of Palaemon macrodactylus: II. association with aquatic bacteria. Biol. Bull. 164: 201-213. Geilenkirchen, W.L.M., Timmermans, L.P.M., Van Dongen, C.A.M. and W.J.A. Arnolds. Experimental Cell Research. 67: 477. Gil-Turnes, M., M. Hay, and W. Fenical. (1989). Symbiotic marine bacteria chemically defend crustacean embryos from a pathogenic fungus. Science, 246: 116-117. Herfurth, A. H. (1936) Bietrage zur Kenntnis der Bacteriensymbiose der Cephalopoden. Z. Morphol. Okol Tiere, 31. Pierantonni, U. (1918). Organi luminosi, organi simbiotici e glandola nidamentale accessoria nei Cefalopodi. Boll, Soc. Nat. Napoli, 30: 30-36. Recksiek, C., and H. Frey. (1965). The structure, development, reproduction, and life history of the squid Loligo Opalescens Berry. Calif. Dept. of Fish and Game Fish Bulletin, 131: 32-63. Spurr, A. (1969). A low-viscosity epoxy resin embedding medium for electron microscopy. J. Ultrastruct. Res., 26: 31-43. Williams, L. (1909). Anatomy of the common squid Loligo Pealii, Lesueur. Brill, Leiden, Am. Mus. Nat. Hist. pp. 51-55. Yang, W.T., R.T. Hanlon, M.E. Krejci, R. F. Hixon, and W. H. (1983). Laboratory rearing of Loligo opalescens, the market squid of California. Aquaculture, 31: 77-88. ZoBell, C. (1946). The antagonistic effects of microorganisms, in Marine Microbiology. (F. Verdoorn, Ed.). Chronica Botanica. c 1.. „ FIGURES Fig. 1. Egg capsules: c-capsule, e-eggs, s-sheath. The capsule on the right has been opened and its contents pulled away from the sheath. Fig. 2. Histological staining of 3 micron sections of freshly laid capsule's sheath show regular striations at 1000x total magnification. Their spacing at 10 to 20 microns implies roughly 100 layers in total. Fig. 3. Bacillus bacteria midway through the depth of the sheath covering a freshly laid capsule - 45,000x. Fig. 4. A shorter rod (a), and the common fusiform morphology (b) midway through the depth of the sheath - 45,000x. Fig. 5a - The vertical bar represents a typical bacterial distribution through the 2 mm depth of the capsule sheath. The water is above/outside, and the eggs below/inside. Distribution of bacteria is distinctly layered. The dark rectangle corresponds to figure 5b. 5b - A typical fluorescence photomicrograph used to map the bacterial distribution depicted in whole in 5a. This is a border between regions of high and low bacterial density, Fusiform sheath bacteria are evident below, stained with DAPI and viewed at 1000x magnification in this optical section through the depth of the sheath. Fig. 6. Striations visible in light microscopy, combined with the fluorescence distribution transect, yield a composite structure: a matrix of fine striations bearing thick, bacteria-laden layers, The dark rectangles, A and B, correspond to figure 2 and figure 5b respectively.