CHEMORECEPTION IN MYXICOLA INFUNDI BULUm Jill Anne Ward June 4, 1976 page 2 Chemoreception in Myxicola ABSTRACI The tubiculous polychaete Myxicola infundibulum has been shoun to utilize chemoreception in connection with its withdrawal response. The worms were found to be expecially sensitive to divalent metal cations such as zinc and copper as they reacted to concentrations as low as 10"'M of these metal ions. Chemoreception in Myxicola page 3 INTRODUCTION Myxicola infundibulum is a sedentary tubiculous poly- chaete which responds to stimulation by rapid withdrawal into its mucus tube (figure 1). The Myxicola escape response has been studied in detail (MoIntosh, 1921; Nicol, 1948, 1955; Roberts, 1962a; Dyal 1972; Binstock and Goldman, 1967, 1969) and has been found to be an extremely rapid all-or-nothing contraction mediated through a single giant axon without synapses and effected by giant muscle fibers running longi- tudinally through the body. Studies done on sensory behavior in sabellids have shown withdrawal responses to tactile stimulation of either the branchial crown or body wall (Roberts 1962a). The reflex has also been obtained from changes in light intensity and shadow movement (Dyal 1972). Chemoreception has been found in several commensal polychaetes in locating hosts (Mackie and Grant 1974), as well as in earthworms (Dyal 1972), and a few errant polychaetes (Mackie and Grant 1974), but it is interesting to study Myxicola's extremely keen sensitivity to chemicals and its use as a possible protection device. Myxicola is particularly good for bioassay due to its clear-cut response, quick recovery from withdrawal, as well as being an easy animal to maintain in the lab. Chemoreception in Myxicola page 4 MATERIALS AND METHODS Specimens of Myxicola infundibulum were obtained from beneath the floats at the Monterey marina. Other invertebrates Used as homogenates in tests were obtained either at the marina or from the intertidal region off Hopkins Marine Station. (see tables 1 and 2). Living animals were kept in running sea water at 12°C. In order to facilitate chemical application. the Myxicola were placed in 2" lengths of glass tubing. which were glued vertically to a Lucite base in a grid for- mation about 14" apart. These tube arrangements were kept in plastic tubs with about thirty worms per tub (figure 2). This separated each worm and allowed all branchial crouns to be faced upward. Several tubs were used to permit rotation of test-worms, thus preventing fatigue. Worms were kept in semi-darkness except when testing, where red light was Used. This eliminated any responses due to change in light intensity or shadow movements, since Myxicola do not respond to red light (Dyal 1972). Disposable syringes with 3" pieces of plastic tubing attached to the ends were used to apply the chemicals, allowing for exact measurement, slow controlled application, little mechanical stimulus, and elimination of the possibility of contamination (figure 3). Animal homogenates were made using approximately 10Omg worm (wet weight) per lml glass-fiber filtered sea water in a mechanically driven Potter-Elvehjem apparatus. Each Chemoreception in Myxice page 5 homogenate was tested at three or more 10-fold dilutions of the initial concentration. The chemicals tested were mixed in molar concentrations and diluted 10-fold from 10*9 to at least 102 molar, except where indicated. Applications were made to interior base of the plume area. The tub water in- flow was turned off to allow for maximum sensory reception, and to minimize dilution of chemicals applied. To eliminate habituation, the worms were tested only once per hour with six tests at most in a given 24 hour period, in accordance with previous studies (Evans 1969, Dyal 1972) EXPERIMENTS AND RESULTS Standardization and Controls The Myxicola were tested with applications of sea water and a mixture of sea water and graphite particles to quantify possible reactions to mechanical stimulus. Fifteen worms were tried with each solution, with only two contractions total. It was almost always possible to distinguish this mechanically-stimulated reaction from a chemical one, however, since the fine-fibered transverse muscles contract uhen Myxicola first is mechanically stimulated, causing the worm to slouly close the end of its branchial crown, and possibly withdraw partially into its tube. Only if the stimulus is increased in magnitude will the giant fibers contract, giving a semi-graded response (Roberts 1962, Dyal 1972). For all page 6 Chemoreception in Myxicola assays in this paper, only rapid and complete withdrawals were counted as positive. Tests were done on Myxicola to determine sensitivity to osmotic and ph changes. The osmotic assay was made using filtered instant ocean (plus trace metals) at concentrations of 50%, 75%, 100%, 150%, and 200% sea water. Worms were also tested with distilled water. Withdrawal responses occured only on application of distilled water, 150% and 200% sea water. PH sensitivity was tested at phs of 3,4,6,and 7 using different dilutions of citric acid; pH 5 with KH,PO,; and pH 7 and 9 using Na,HPO,. 60%-100% worms were sensitive to acidic phs (especially citric acid), but less than 20% were receptive to alkaline pH. Effects of Animal Homogenates Homogenates of several invertebrates from both the same habitat as Myxicola (the marina) and also a different one (intertidal) were assayed to compare Myxicola's sensitivity to different animals as well as find out whether the chemical might be species specific or habitat specific, or possibly due to a predator-prey situation (see tables 1,2.3). An observation of a live arabellid specimen with a Myxicola placed together in a fingerbowl for several minutes revealed that the withdrawal response was not effected by the presence of a live arabellid. page 7 Chemoreception in Myxicola Next, several tests were done using the arabellid homogenate to characterize the compound active in causing Myxicola's withdrawal. A homogenate solution made up of .omg (wet weight) arabellid plus 6ml filtered sea water was centri- fuged for 15 minutes at 1500 rpm. Activity was found in both the clear supernatant (80% at .6% solution conc. - .0216 mg dry arabellid per ml sea water) and in the sediment (not quantified). The homogenate was dialysed in a rotating dialyser for 48 hours at 6°C, using a Spectrapore membrane tubing bag (type 2: m.w. cutoff 12,000-14,000) and five outer volumes. The inside and outside solutions were freeze-dried and reconsti- tuted to their original water concentration and osmolarity for the assay, which showed the chemical to be dialysable (at 1% dilution, 80% Myxicola reacted to outer solution, 10% reacted to inner solution). An assay was also done for heat stability. An arabellid was dried in an oven for 8 hours at 76°C. and then made into a solution and centrifuged. The supernatant yielded an 80% reaction at .8% dilution (=.0245mg dry weight per ml sea water). The arabellid homogenate was also tested for stability against oxidation. 30% H,O, was added in excess to a solution of .5mg worm per ml sea water, then the H202 was evaporated and the solution reconstituted. The assay resulted in an 80% reaction at 1% concentration of solution (- .18m9/ml sea water) Chemoreception in Myxice page 8 Arabellidae is a family closely related to Lumbriconereis which has been found to contain nereistoxin' (Deguchi, Nara- hashi, Haas 1971). The arabellid homogenate was tested on frog rectus abdominus muscle for any possible inhibition of the effect of acetyl choline. Several trials yielded no decrease in the muscle's sensitivity to acetyl choline. Acetyl choline w as also applied to live Myxicola, as was carbachol, but both these chemicals failed to elicit the withdrawal response at concentrations of 1 mg/l0ml sea water! Effect of Known Chemicals In the next approach, assays of known chemicals (of characteristic types) were made in an attempt to find out what chemical or class of chemicals Myxicola might be sen- sitive to (tables 4 and 5). Methylene blue (graph 5) was tested before use as a color- ing agent in the assay of clear amino acid solutions, but was found to elicit a reaction in Myxicola at very low con- centrations. Since zinc chloride is known to be an impurity in the methylene blue staining solution, it and several (rauxe) other transition metals were tried on the Myxicola. Very clear positive results were obtained at strikingly low con- centrations of the metals. (Myxicola is much more receptive nereistoxin is a naturally occuring toxin which blocks the stimulatory action of acetyl choline on smooth muscle fiber. Chemoreception in Myxice page 9 to these chemicals than any others tried so Far.) Myxicola reacted to several similar metals, but had different degrees to sensitivity to different metals. The tunicate with which Myxicola is closely associated (Ascidea ceratodes) at the marina concentrates vanadium, (Goldberg 1970) another divalent metal, so a solution of Ascidea blood and 10-fold dilutions of it were tried (graph 7). It is interesting to note however, that the solutions of V2Ug and Batl, were not especially active in eliciting the Myxicola response. DISCUSSION he experimental results clearly show that Myxicola conclusively employs chemoreception as another means of sensing the environment. Preliminary tests show the active compound to be naturally occuring, at least partially free in solution, fairly small in molecular weight, heat stable. and stable against oxidation. All these characteristics readily support the data showing Myxicola's sensitivity to metal cations. The positive reactions to mixtures of organic substances can also be explained in this way since many of the chemicals asaayed (i.e. casein hydrolysate) are known to contain trace amounts of metals to which Myxicola is so sensitive. Two possible reasons for this sensitivity have to do with Myxicola as prey, and Myxicola's adaptation to a polluted environment. page 10 Chemoreception in Myxicnla Myxicola live at the marina in amongst many other in- vertebrates, some of which are known to concentrate certain metals in their bodies (Goldberg 1970). A tunicate, Ascidea ceratodes, is abundant at the marina and concentrates vanadium in its blood. The scyphistoma stage of Lyanea capitella has also been seen in the same environment (Abbott 1976) and concentrates copper (Goldberg 1970). Myxicola's positive reactions to several dilutions of Ascidea blood might lead to the possibility of a sympathetic withdrawal due to the sensing of an injury in a neighboring animal. The idea of metal sensitivity as a defense against pollution is another possibility. Several of the metals meas- ured are known to be toxic to marine invertebrates in higher concentrations (Portmann 1972). A response to a slight increase in metal would enable Myxicola to withdraw into its tube in case dangerous amounts of toxic metals were diffusing through the water. These ideas are beyond the scope of this project, however, but any possible adaptive sensitivity would be advan- tageous for Myxicola's protection and is worth considering. It is also interesting that homogenates from animals not from the same environment as Myxicola generally had the same effect on Myxicola as animals from the same habitat. This rules out the possibility of the chemoreception being specific between a predator and prey, and the widespread acivity clearly eliminates the possibility of the chemical being a species specific pheromone. Chemoreception in Myxicol: page 11 Since the chemicals had to be applied to the interior base portion of the branchial croun to be effective in the assay, it is assumed that the chemoreceptors are located in this area. This is supported by the fact that nereids have been found to have chemoreception in their prostomial cirri (Laverack 1974), which correspond closely to the small tentacles at the end of Myxicola's prostomium. Leherally, Myxicola has been shown to be a good, consistant bioassay for several metals. In addition to responding immediately to the stimulus, the recovery time is very short. and accomodation to repeated stimuli is relatively slow. page 12 Chemoreception in Myxicola ACKNOULEDGMENTS I would especially like to thank Dr. F.A. Fuhrman for all his extremely invaluable assistance in this research, and Dr. Robin Burnett and Chuck Baxter for their encouragement and criticism. Thanks also to Gordy Kauhanen for helping with the set-up design, and to the entire class and faculty for making my experience at Hopkins so terrific. Chemoreception in Myxicola page 12 REFERENCES Abbott, D.P., Personal Communication Binstock, L. and L. Goldman (1969) Current and Voltage-Clamped Studies on Myxicola Giant Axons, J. Gen. Physiol. 54: 730-741 Binstock, L. and L. Goldman (1967) Siant Axon of Myxicola: Some Membrane Properties as Observed Under Voltage Clamp Science, 158: 1467-1469 Deguchi, Narahashi, Haas (1971) Mode of Action of Nereistoxin on the Ne romuscular Transmission in the Frog. Pesticide Biochem. and Physiol. 1: 196-204 Dyal, J.A. (1972) Behavior of Annelids, Report 441 University of Waterloo Research Reports in Psychology Evans, S.M. (1969) Habituation of Withdrawal Response in Nereid Polychaetes Biological Bulletin 137: 105-117 Goldberg (1970) Review of Trace Element Concentrations In Marine Organisms Puerto Rico Nuclear Center Laverack, M.S. (1974) The Structure and Function ofChemoreceptor Lells p1-48 in"Chemoreception in Marine Organisms"(Grant and Mackie, eds.) London, Academic Press Chemoreception in Myxicola Page 13 Mackie, A.M. and P.T. Grant (1974) Interspecies and Intraspecies Chemoreception by Marine Invertebrates, p 105-141 in Chemoreception in Marine Organisms"(Grant and Mackie, eds.) London, Academic Press MoIntosh, W.C. (1921) A Monograph of British Annelids, vollV,ii London, Dulau & Co., p307-310 Nicol, J.A.C. (1948) The Giant Nerve-Fibers in the Central Nervous System of Myxicola (Polychaeta: Sabellidae) Quart.J. Micro. Sce. 89:1-45 Nicol, J.A.C. and Whitteridge (1955) Conduction in the Giant Axon of Myxicola, Physiol. Comp Oecol. 4: 101-117 Portmann, J.E., Loxicity Testing with Particular Reference to Oil-Removino Materials and Heavy Metals, in "Marine Pollution and Sea Life" (Ruivo, ed.) p 217-221 Roberts, M.B.V. (1962a) The Rapid Response of Myxicola (Grübe) J. Mar. Bio. Ass. 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