Uptake of C+0, and C glycine by zooxanthellae and Anthopleura elegantissima Richard M. Leonard* Abstract--1. C+0, and C-glycine are both incorporated into the free amino acids of Anthopleura elegantissima and its zooxanthellae. 2. C+ is incorporated in greater concentration by zooxanthellae than by Anthopleura elegantissima Introduction The uptake of C labelled substances and the subsequent transference of C+ labelled photosynthetic products by endozoic zooxanthellae to their coelenterate host has been demonstrated in the Zoanthid Zoanthus flosmarinus (von Holt and von Holt 1968a). In subsequent study if was shown that the endozoic zooxanthellae were unable to synthesize their own glycine when given COg or when given serine which is the immediate precursor in the glycine synthetic pathway (C. von Holt 1968 ). Using " radio-tracer" methods it was shown (C. von Holt 1968 ) that zooxanthellae preferentially incorporated over other amino acids C labelled glycine into their amino acid pools, indicating a possible specific metabolic interaction in the Zoanthus-zooxanthellae symbiotic relationship. These observations prompted a study of the dynamics of CO, and glycine uptake in the Actinaria Anthopleura elegantissima to see if there was any similarity to the dynamics of Zoanthus flosmarinus. Materials and Methods Specimens of the experimental animal Anthopleura elegantissima were collected from the intertidal region of Mussel Point in Pacific Grove California. Oral discs of all the specimens were between 3 and 4cm in diameter at maximum expansion. Animals were kept in running seawater prior to experiments. The isolation procedure of the zooxanthellae from the coelenterate was that of von Holt and von Holt (1968a). *Present address: 2891 Dellwood Dr. Lake Oswego, Oregon 97034. Glycine and Anthopleura elegantissima -2- For incorporation experiments three organisms of Anthopleura elegantissima were allowed to settle onto the inside of lids of 50ml glass jars. The jars were each filled with 40ml of fresh seawater, to which was added lmicroCurrie of respective C source (either Nac-0, or C+-glycine (Universal Label-New England Nuclear Corp.)). The lids containing the coelenterates were put on the jars and the jars were inverted and placed under a bank of flourescence lights (150 foot-candles) and incubated for four hours. After incubation the animals were washed in fresh seawater and the algal and animal cells separated as described by von Holt and von Holt (1968a). After separation both the animal and the algal fractions were boiled in 250ml of 85% ethanol for two hours. The insoluble portion was removed via centrifugation, the soluble portion was mixed with 200ml of petroleum ether, and the aqueous layer was removed and reduced in volume by boiling to 5ml. This I called the "amino acid fraction! An aposymbiotic specimen of Anthopleura elegantissima was also incubated under the same conditions and its "amino acid fraction was similarly extracted. Zooxanthellae isolated from three specimens of Anthopleura elegantissima of the 3-4cm size were incubated in 40ml of fresh sea¬ water as described. An "amino acid fraction" was prepared in the manner described. 250 microliters was taken from each of the "amino acid fractions added to 10ml Aquasol universal liquid scintillation cocktail (New England Nuclear Corporation,mfg.) and counted in a Unilux II scintillation counter for one minute. 250microliters of each "amino acid fraction" was dried and weighed. For each sample a ratio of C activity to weight of dry "amino acid fraction " was determined, expressed in units of microci/gram. This ratio was then used as a means of comparing the C uptake of different " amimo acid fraction' samples. Results The results are summarized in table 1. Anthopleura elegantissima incubated in seawater in the presence of labelled carbonate incorporates C+0, into the "amino acid fraction " of the algal cells as well as the animal cells( Table 1,samples 1 and 2 ). In samples 1 and 2 the zooxanthellae incorporated more C+ than the host Anthopleura elegantissima. C -glycine was also incorporated into Glycine and Anthopleura elegantissima -3- the algal cells and into the animal cells (Table 1, sample 3). Sample 3 also incorporated more label into the algal cells than into the animal cells. Discussion Endozoic zooxanthellae are widely distribued in marine organisms particularly in coelenterates (Droop, 1963). That the zooxanthellae release organic material into the incubation medium under in vitro conditions has been demonstrated by the work of von Holt and von Holt (1968a,b) and by Muscatine( see Muscatine 1974). In von Holt and von Holts work with Zoanthus flosmarinus (1968a,b) the in vivo incorporation of photosynthetically assimilated C into the animal matrix was evidence that the coelenterate host utilized products released by the zooxanthellae. My results may indicate similar in vivo utilization by Anthopleura elegantissima. Of particular interest is the comparison of C 0, and C- glycine uptake. In samples 1 and 2 the ratio of C incorporation in the algal cells and animal cells is approximately 1.4:1 whereas in sample 3 the ratio is approximately 5:1. The greatly increased ratio resulting from C-glycine uptake may result from the zooxanthellae in Anthopleura elegantissima being unable to synthesize their own glycine and thereby incorporating it in large concentration when available. CO, enters through the animal tissue, goes to the algal cells where it is acted upon photosynthetically and some of the labelled photosynthetic products are released back to the coelenterate host. When Cglycine is the source the photosynthetic abilities of the algal cells are not needed for conversion and inorporation of( " into the algal and animal cells. This fact, the fact that the C source must go through animal tissue to be incorporated by the algal cells, and the 5:1 C+-glycine uptake ratio previously eluded to may indicate that glycine occupies an important role in Anthopleura elegantissima symbiosis. The metabolic relationship between Anthopleura elegantissima and its endozoic zooxanthellae is obviously complex. Moreover there may be important differences in the metabolic activities of the zooxanthellae isolated from different Anthopleura elegantissima, as well as metabolic differences in the host. The dependence of the algal metabolism on glycine from Anthopleura elegantissima would play an important role in the symbiosis of Anthopleura elegantissima and its zooxanthellae. Glycine and Anthopleura elegantissima -4- References Droop M.R. (1963) Algae and invertebrate in symbiosis Symp. Soc. gen. Microbiol. 13, 171-199 Muscatine L. (1974) Coelenterate Biology Reviews and New Perspectives pp. 376-389, Academic Press, New York. von Holt C. and von Holt M. (1968a) Transfer of photosynthetic products from zooxanthellae to coelenterate hosts. Comp. Biochem. Physiol. 24,83-92 von Holt C. and von Holt M. (1968b) The secretion of organic compounds by zooxanthellae isolated from various types of Zoanthus. Comp. Biochem. Physiol. 24,73-81 von Holt C. (1968) Uptake of glycine and release of nucleoside¬ polyphosphates by zooxanthellae. Comp. Biochem. Physiol. 26, 1071-1079 Acknowledgements Thanks to everyone involved with 175H, it was a great quarter. Special thanks to Robin Burnett for his help and patience. sample + Glycine and Anthopleura elegantissima Table 1 cell source C source C+ activity cell type .o026 animal symbiotic co .0038 co plant symbiotic 00 animal symbiotic .0015 plant co .0020 symbiotic 0044 animal symbiotic glycine symbiotic plant glycine 0213 isolated from plant 00 .0032 symbiotic co aposymbiotic .O010 animal isolated from plant symbiotic co .0033 isolated from .0107 glycine plant symbiotic e Table 1. Glycine and Anthopleura elegantissima -6- Caption for table + activity of Anthopleura elegantissima and zooxanthellae (microCurries/gram of dried amino acid fraction"). 0