E. Kincannon Temm rature Response in Tonicella Page 0 Abstract Two vertically separated populations of Tonicella neata (Wood) were tested for acute and acclimated res¬ piratory rates at a series of five temperatures. Oxygen uptake was considered as a function of both body weight and temperature. Q in these chitons was not affected by body weight. Intertidal Tonicella were shown to have a greater ability to compensate for temperature changes than the subtidal population; they showed better acclimation patterns after three weeks in the laboratory and showed decreasing 0's at higher temperatures while 0 of the subtidal population remained constant. These results are related to stability of temperature regimens in each habitat. Temperature Response in Tonicella E. Kincannon page 2 INTRODUCTION Intertidal molluscs are known to show compensatory changes in metabolic rate in response to different temperature regimes. For example, some species from high latitudes have the same rates of oxygen consumption as do related tropical species at warmer temperatures (see reviews by Bullock, 1955, and Segal, 1961). Furthermore, this compensation, or acclimation, has been shown between two spatially separated populations of the same species. Low level populations of the limpet Collisella limatula (Carpenter, 1864) show cold acclimation of heart rate while high intertidal C. limatula from a few feet away show warm acclimation (Segal, 1956). Kenny (1958) suggests that this should apply to the Poly- placophora as well; the chiton Clavarizona hirtosa (Blain¬ ville) from low intertidal zones shows a lower upper lethal temperature than those from comparatively higher, warmer zones. However, no definitive work on acclimation as a function of microgeographic separation has been done on the Polyplacophora. This study was designed to answer the following questions: (1) Can chitons acclimate to altered temperatures within a few weeks? (2) If so, are subtidal animals acclimated to a lower temperature than intertidal ones of the same species; (3) Are intertidal animals, which are exposed to E. Kincannon Temperature Response in Tonicella wide fluctuations in habitat temperature, better able to acclimate to experimental temperatures than subtidal ani¬ mals, which experience a more limited temperature range? The species Tonicella lineata (Wood, 1815) was selected for study because of its wide vertical distribution. In addition to being abundant subtidally (Barnes, 1972, p. 67). the species has been found by the author to occupy sides in the intertidal up to three feet above mean lower low water. Exchange of individuals between deepwater and shallow pop¬ ulations is probably small or nonexistanat (Demopulos, 1974). Acute respiratory rates (oxygen consumption rates of animals collected and held at constant temperature for one day before measurement) were compared with rates of acclimated aniamls (held three weeks at constant temperature prior to measurement), at a series of five temperatures. Rate of oxygen consumption was used as an indicator of metabolic rate. Since many factors other than temperature affect respiratory rate, notably body weight and activity level, an attempt was made to study and correct for these variables. There is evidence (Bullock and Rao, 1954) that temperature affects the relationship between body weight and respiratory rate. Consequently, weight-rate regressions were done at each temperature for each population, using the formula M = k-W. Where M = metabolic rate, K = a constant, W - weight of the organism, and b - the regression coefficient. page 3 E. Kincannon Temperature Respe in Tonicella page 4 MATERIALS AND METHODS All intertidal Tonicella were collected from Carmel Point, Carmel, California, between O and 2 feet above mean lower low water. Subtidal Tonicella were collected at a depth of 20 to 26 feet off Mussel Point, Pacific Grove, California. In the laboratory, all were held under constant light in aquaria equipped with air stones. Constant temperature was maintained by means of running sea water and immersion heaters. Three holding tanks were maintained in this manner at 8°C, 13°C, and 18° C; temperature was checked daily and fluctuated + 2°C in the two warmer tanks, less in the 8°C tank. Large glass jars covered with plastic screens served both to keep the chitons submerged and to keep the popula¬ tions separate. Rates of oxygen consumption were expressed on the basis of wet weight which was measured by blotting the Tonicella with paper towels before weighing. Fourteen chitons were weighed after 29 hours in an 80°C oven. They were then combusted at 600°C for 48 hours. Those initially weighing over 2 g were combusted 6 days and reweighed. Percentages of dry to wet weight, and ash-free to dry weight, were subsequently calculated and plotted as a function of wet weight. Rates of oxygen consumption were measured at experimental temperatures of 3°c, 8°c, 13°C, 18°C and 23°C using the direct E. Kincannon Temperature sponse in Tonicella page 5 Warburg method of constant volume manometry as described by Umbreit et al. (1972). After collection, Tonicella were kept in the holding tank closest in temperature to that at which they would be tested. Before the experiment they were weighed, placed in the Warburg reaction vessel, and covered with a measured volume of sea water filtered through a 0.22 u Millipore filter. Oxygen consumption by particles less than 0.22 u was assumed to be negligible. Two-tenths of a ml of 10% KOH was added to a filter paper wick located in the side¬ arm. After one hour of equilibration in the water bath, manometer readings were taken at one-hour intervals for six to twelve hours, depending upon the time required for respiratory rates to stabilize. Hourly rates of oxygen uptake were calculated and averaged over the time interval showing the most consistent rates. Notes on the animals' activity and degree of submersion were kept throughout each experiment. Only the rates of those chitons which appeared unhurt, remained submerged, and did not move more than a few cm were used in further calculations. Each chiton was used in only one experiment, after which it was liberated. Acute respiratory rates were measured 22 to 26 hours after collection for six Tonicella at each temperature. Rates of acclimated animals were measured after three weeks using two specimens for each combination of acclimated and experimental temperatures. A regression analysis was performed on each set of acute rates measured, using a double E. Kincannon Temperature Response in Tonicella page 6 logarithmic transformation (Sokal and Rohlf, 1969). The method of least squares (Ibid., Box 14.1) determined the regression coefficients, and Fisher's F-test (Ibid., Box 8.1) tested the significance of the lines. In the comparison of regression lines with each other, the F-test was used to compare slopes (Ibid., Box 14.8), while Student's T-test (Ibid., Box 9.6) compared the means after a determination that the variances were similar (Fisher's F-test as above). The mean weight of all chitons collected was 0.70 g. Rates of oxygen consumption for this weight were obtained from the regression line at each temperature and plotted on a rate vs. temperature graph. Assuming that b, the slopgof the regression line, remains constant with acclimation, rates of acclimated animals were standardized to this same weight and plotted with the same procedure as the acute rates. Since all rate-temperature curves were plotted semilogarithmically, their slopes are directly pro¬ portional to Qjo as calculated by the formula: Ri 10/t-t) 210 - R9 (Prosser, 1973, p. 363). RESULTS AND DISCUSSION Wet weight as a measure of metabolizing tissue Figure I shows dry weight as a percentage of wet weight and ash-free dry weight as a percentage of dry weight for a nearly fifty-fold range of weights of Tonicella. Apparently Temperature Response in Tonicella page 7 E. Kincannon the proportion of water (upper graph) and ash-weight (lower graph) in Tonicella does not depend upon total wet weight. Ash-free dry weight excludes the bulk of a chiton's normetabolizing tissue—the shell plates. However, other non-metabolizing elements such as fats and connective tissue will combust and thus form part of the ash-free dry weight. These could conceivably be present in larger amounts in larger animals, leaving less metabolizing tissue in proportion, and thus contribute to an overall decrease in weight-specific metabolism in larger creatures. However, ash-free dry weight has commonly been used as a measure of the amount of metabolizing tissue in an organism. Since ash-free dry weight represents a fairly constant proportion of weight weight. I chose to compute weight-specific respiration in terms of wet weight. Stability of respiratory rates To determine whether respiratory rates measured over a 6 to 12-hour period are representative of an entire 24-hour period, five chitons were tested for 24 hours. Change in manometric pressure is plotted against time in Figure 2. Although many species show a diurnal or tidal respiratory rhythm, this is clearly not the case for Tonicella. (The irregularity near 0800 hours was reflected by the thermo¬ barometer and is not due to changes in respiration.) E. Kincannon Temperature Response in Tonicella page 8 Effect of body weight upon respiratory rate Rates of oxygen consumption as a function of body weight at five different temperatures in subtidal and intertidal populations are plotted in Figures 3 and 4 respectively. Slopes and 95% confidence limits for each regression line appear in Table 1. Correction for weight by means of regression analysis greatly reduced the variance in even these small samples of rates; this suggests that at any given temperature, weight is a more important determinant of respiratory rates in Tonicella than are other factors such as sexual and nutritional states. Statistical comparison of the regression lines revealed no consistent pattern of change in the slopes (b-values) as a function of termperature. The slopes of subtidal animals (Table 1) suggest a pattern of decreasing b-values with decreasing temperature, but this is not a statistically significant trend and does not appear in the intertidal population. It may be concluded from this that b for this species does not change with temperature, large and small Tonicella are equally affected by temperature, and Q0 does not vary with size. These conclusions represent an exception to the general rule. For example, in intertidal invertebrates studied by Edwards and Irving (1943), Bullock and Rao (1954) and Newell (1970). b decreased with temperature and 9, decreased with body weight. The results presented here for Tonicella are therefore quite significant, and need to be confirmed with more data and clearer statistical conclusions. Temperature Response in Tonicella page 9 E. Kincannon These data also suggest that vertical location does not affect the relationship between body weight and respiratory rate; there are no consistent differences in b between sub¬ tidal and intertidal Tonicella tested at the same temperature. An average of all 10 slopes obtained yields a b-value of 0.73 for this species. This is similar to those of other molluscs as reported by Prosser (1973, p. 193) and close to Zeuthen's (1970) generalized metazoan value of 0.74. Effect of temperature upon acute respiratory rate Figure 5 shows acute rates of oxygen consumption for a hypothetical 0.70 g chiton plotted against temperature. These points are derived from the regression lines in Figures 3 and 4, and their significance is determined by the confidence limits of those lines. It is apparent that the curve for intertidal Tonicella does not lie below that for subtidal Tonicella. Subtidal chitons therefore do not appear to be cold-acclimated; these results suggest that they may even be warm-acclimated since their rates are generally lower than those of the intertidal population. Althought this seems unlikely, the question cannot be resolved until it is known to what aspect of the thermal regime these animals are responding. According to temperature data from nearby Moss Landing, California (Harrold, Christopher personal communication, 1974), intertidal animals are frequently exposed at low tide to air temperatures both higher and lower E. Kincannon Temperature Response in Tonicella page 10 than that of the ocean. If they are acclimating to the lowest temperature in their environment, they could indeed appear cold-acclimated in comparison with subtidal chitons. Vernberg and Vernberg (1970, p. 132) have suggested that the temperate-zone crabs Uca pugnax (Rathbun, 1901) are better able to adapt to temperature extremes than are their tropical relatives Uca rapax (Rathbun, 1918) because they are exposed to more temperature fluctuations. This argument may apply to Tonicella in that subtidal chitons are exposed to a more narrow temperature range and would be expected to be less flexible in respiratory response than intertidal ones. From Figure 5, subtidal Tonicella show a a constant 0l0 near 2.5, while intertidal ones appear to decrease their Olos in higher temperatures. Segal (1956) has found similar patterns in his work with heart rate in Acmaed, although Bullock and Rao (1954) stated that Oho generally increases with temperature in molluscs such as Mytilus salifornianus (Conrad, 1837). Since a lower 0 would be advantageous for an intertidal animal exposed at midday low tide to the sun, this preliminary result should be further tested by repetition of these experiments, including teperatures higher than 239c. kelation of acclimation to temperature Rates for each population of acclimated Tonicella corrected to a standard body weight using acutely measured E. Kincannon Temperature Response in Tonicella b values are plotted in Figure 6. Very little can be said about the subtidal population (Figure 6-B) because of the intertwining curves. However, it appears that acclimation has occurred to some extent in the intertidal population (Figure 6-A). The rate-temperature curve for 13°0 acclimated animals falls below that for 8°C acclimated aniamls at all points, although the distinction between 13°C and 18°C curves is less clear. This is probably due to greater temperature fluctuations in the two warmer tanks than in the 8°C holding tank. These results come after a relatively short period of acclimation, and experiments conducted for a longer time are necessary to determine whether or not subtidal Tonicella in fact can acclimate. Nonetheless, they support the argument of the preceding section that intertidal Tonicella are capable of compensating for changes in their environmental temperature and possibly can do so better than the subtidal Tonicella. The curves in Figure 6-A do not show the same pattern of decreasing Q with increasing temperature as do the acutely measured rate-temperature curves. However, the absolute shape of these curves is not as accurate, since only one or to experimental animals determined each point and b-values were not measured for acclimated animals. The curves in Figure 6 are useful only in comparison with each other. There remains the possibility that acclimation observed page 11 E. Kincannon Temperature Response in Tonicella in the laboratory is due to factors other than temperature. Starvation is an obvious possibility; Newell (1970, p. 391) reports that this is common and results in a decrease in respiratory rate. However, at least one group of intertidal Tonicella (8°c-acclimated, tested at 23°C) had higher rates than did thecorresponding acutely measured group, and the Tonicella were observed to deficate fecal pellets through¬ out their three weeks in the holding tanks. Possibly more variation would have been introduced by trying to feed the Tonicella than by starving them. Future studies An interesting question remaining is whether or not b changes with laboratory acclimation. For the purposes of this project no change was assumed, but this need verification. Another topic is that of standard vs. active metabolism and its effect on 9,: the 0,s found in this project are higher than those given by Newell (1970) for standard metabolism. Finally, once it has been determined that a population of Tonicella can acclimate, transplantation experiments would be helpful to test whether animals from one habitat can acquire the ability to acclimate over a short period of time. SUMMARY 1. Two vertically separated populations of Tonicella lineata pagel2 E. Kincannon Temperature Response in Tonicella page 13 (Wood, 1815) were tested for acute and acclimated respiratory rates at a series of five temperatures. 2. Tonicella show no diurnal or tidal rhythm in respiratory rate. seems unaffected by body weight in both populations. 3. 0, 4. Subtidal Tonicella are not acclimated in the field to a colder temperature than are intertidal Tonicella, but may be less able to compensate for temperature change. 5. Intertidal Tonicella show a pattern of acclimation after three weeks in the labotatory; results from subtidal animals are ambiguous. ACKNOWLEDGMENT I wish to thank Dr. Fred Fuhrman and Paul Boothe for their assistance and advice on this project. I greatly appreciate the faculty, students, and staff of Hopkins Marine Station for creating a friendly and stimulating at atmosphere in which to work. Special thanks are reserved for Chris Harrold, my advisor, for his guidance and infinite patience. E. Kincannon Temperature Response in Tonicella page 14 LITERATURE CITED Barnes, James Ray 1972. Ecology and reproductive biology of Tonicella lineata (Wood, 1815) (Mollusca--Polyplacophora). Ph.D. dissertation. Dept. of Zoology, Oregon State University. 161 pp.; 47 figs. (June 1972) Bullock, Theodore Holmes 1955. Compensation for temperature in the metabolism and activity of poikilotherms. Biol. Rev. 30 (3): 311-342; 5 figs. (1 June 1954) Bullock, Theodore Holmes, and K. Pampapathi Rao 1954. 010 as a function of size and habitat inpoikilotherms. Amer. Natur. 88: 33-44; 7 figs. Demopulos, Peter Andrew 1974. Diet, activity and feeding in Tonicella lineata (Wood, 1815) with notes on its taxonomy. The Veliger Edwards, G. A., and Laurence Irving 1943. The influence of temperature and season upon the oxygen consumption of the sand crab, Emerita talpoida Say. Journ. cell. comp. Physiol. 21 (2): 169-182; 4 figs. Kenny, Ron. 1958. Temperature tolerance of the chiton Clavarizona hirtosa (Blainville). Journ. Roy. Soc. West. Aust. 41 (4) : 93-101; 6 figs. (1 January 1958) Newell, Richard Charles 1970. Factors affecting the rate of oxygen consumptinn. 3/2-450 in R. C. Newell, Biology of intertidal animals E. Kincannon Temperature Response in Tonicella page 15 New York, N.Y. (American Elsevier, Publishing Co., Inc.) Prosser, Clifford Ladd, ed. 1973. Comparative animal physiology. Vol. I. 3rd ed. xxii + 456 + xlv pp.; illus. Philadelphia, Penna. (W. B. Saunders, Co.) Segal, Earl 1956. Microgeographic variation as thermal acclimation in an intertidal mollusc. Biol. Bull. 111(1): 129- 152; 8 figs. Segal, Earl 1961. Acclimation in molluscs. Amer. Zoll. 1: 235-244: 5 figs. (12 Dêcember 1960) Sokal, Robert R., and F. James Rohlf. 1969. Biometry. xxi + 776 pp.; illus. San Francisco, Calif. (W. H. Freeman and Co.) Umbreit, W. W., R. H. Burris, and J. F. Stauffer 1972. Manometric and biochemical techniques. 5th ed. v + 387 pp.; 125 figs. Minneapolis, Minn. (Burgess Publishing co.) Vernberg, F. John, and Winona B. Vernberg 1970. The animal and the environment. xv + 398 pp.: illus. New York, N. Y. (Holt, Rinehart and Winston, INC.) Zeuthen, E. 1970. Rate of living as related to body size in organisms. Polskie Arch. Hydrobiol. 17(30): 21-30; 7 figs. E. Kincannon Temperature Response in Tonicella TABLE CAPTION Table 1. Statistics for the weight regression lines shown in Figures 1 and 2. Values are based on a double logarithmic transformation. Ninety-five per cent confidence limits for the y values (rates) are obtained by constructing parallel lines at a vertical distance of 2's above and below the regression line on log scale. Temperature Response in Tonicella E. Kincannon FIGURE CAPTIONS Figure 1. Relationship between wet, dry, and ash-free dry weights in selected Tonicella lineata of various sizes. Upper plot is dry weight as a percentage of wet weight; lower plot is ash-free dry weight as a percentage of dry weight. Figure 2. Respiratory rates of Tonicella lineata measured over a 24-hour period. Change in manometer reading as plotted is proportional to oxygen consumption. Weights are those of the chitons tested. Figure 3. Oxygen consumption as a function of body weight for subtidal Tonicella lineata. Rates were measured at five temperatures 24 hours after collection. Each point represents one animal. Figure 4. Oxygen consumption as a function of body weight for intertidal Tonicella lineata. Rates were measured at five temperatures 24 hours after collection. Each point represents one animal.. Figure 5. Rate vs. temperature curves for intertidal () and subtidal (0) Tonicella lineata, measured acutely. Points represent the intersection of a perpendicular, erected at 0.70 g, with weight regression lines at each temperature. E. Kincannon Temperature Response in Tonicella Figure 6. Rate vs. temperature curves for intertidal (A) and subtidal (B) Tonicella lineata acclimated to various temperatures in the laboratory for three weeks. (8°C -2 13°c -+, 18°c -2). Each point is the mean of two animals, corrected to a standard weight of 0.70 g as in Figure 5; vertical lines represent the range. E. Vronne Orgweight wet weight 0 + 80 fr. 2. K 47.9 — 17 20 oto+ en-5. 50- ash-Tree digweght 40 + drg weight — o8a ao 24 28 3.2'30 40 Wer weight (g) 90 F. KinbéANN .259 ol -- (0 + -363 § 20— a 10 — .679 0 C t.429 1e 3.489 3 §791 lan.3 S 7 à 1 10.m. Time of Oaq Eigore 2 E. Wesre 10 — 08 + 06 1 0 + .02 O.01. oo- 00 7— o 003 237 130. . 280. 6 —1— 4681o 10 30 4.0 Wet Weigh+ (g) Figore 3 .2 E Rionannon 10— .06- .041 2 8 -02 + 01 o0- o07- 05 003 + . 2 2 230 e fge. + 6.810 2.0 3.0 4.0 et wegh+( ore 0 E Kinore 83 8 0 50151 60 003 - o 13° (2° 23. Temperatore (°c.) Fgore 6 05 03 ol 0161 008 + 00 f. Kincr 8 13 18 23 Temprator ( Fgoret 8 —— 13 18 23 B. e Temprature Response in Tonicella . Kincannon Table 1 -------------------------------------------------—-------- ropulation Subtidal Interidal —----------- —-- ------------ ---- —----------------- Terperature 38. 10%. 8%. 188 8° 32c. ------------------------------------------------------- .70.69 .86 .80 .59.68 .80 .57 .01 .81 -------—--------------------L---L---- 5 Conl. mits .151.085.032 .166.138 .089.121 .050.180 .251. 2.S ------L--------------------------- — — — -