Rollins 1998 Abstract This project focused on the development of an anesthetic regimen in yellowfin tuna (Thunnus albacares), bonito (Sarda chiliensis), and Pacific mackerel (Scomber japonicus), while monitoring effects on blood chemistry and hematology. Anesthesia was induced with a combination of ketamine and medetomidine, and compared to MS- 222 (3-amino benzoic acid ethyl ester). Ketamine and medetomidine were injected into the red muscle of fish, while MS-222 was applied by immersing a fish in a drug and seawater solution. Effects of anesthesia were monitored and blood samples were taken. Blood was then analyzed for hematocrit, hemoglobin, enzymes, metabolites and ions. Survivorship between the species varied, with yellowfin tuna at 0% survival and bonito the highest at 50% survival. A trend relating an increase in time of the anesthetic induction period to decreasing metabolic rate was noted. Additionally. time until recovery from anesthesia was found to increase with the ratio of ketamine to medetomidine in yellowfin tuna, but was found to decrease with the ratio of the two drugs in bonito. Anesthesia was found to have no effect on average yellowfin tuna hematocrit (mean level = 33.4 +2.2). However, a positive relationship between yellowfin tuna hematocrit and medetomidine dose was noted (r2-0.83). A negative relationship between bonito hematocrit and the ratio of ketamine to medetomidine was also present. A significant increase in ions (calcium, chloride, potassium and sodium) and some enzymes (aspartate aminotransferase and creatine phosphokinase) was noted in yellowfin and was most likely due to the high levels of activity associated with anesthesia. Further studies into this form of intramuscular anesthesia are needed, both to better determine the feasibility of usage of the drugs in yellowfin tuna, and to ascertain an ideal anesthetic dose in bonito and mackerel. page 2 Rollins 1998 Introduction Research on wild and nondomestic vertebrates has contributed significantly in many fields, from ecology to physiology and microbiology. However, this research can require sedating animals, or applying a form of analgesia. A regimen of anesthesia is an ideal tool in vertebrate research, as it often provides both sedation and analgesia. This project focused on the development and utilization of an anesthetic regimen in scombrids: yellowfin tuna (Thunnus albacares), bonito (Sarda chiliensis) and Pacific mackerel (Scomber japonicus). A primary goal of this work was to determine the specific dosage of an intramuscular anesthesia for the three species of fish, while monitoring the physiological effects of anesthesia through blood chemistry and hematology. Interest in anesthetization of scombrids came about due to their commercial and scientific importance. As major targets of global fisheries, research into their behavioral patterns and physiological characteristics is of utmost significance. The fast-moving tuna is also an anomaly among fish, due to its partial endothermy and high metabolic rate (Brill 1987, Carey et al. 1971). The unique physiology of tunas makes the study of yellowfin tuna important from a variety of physiological and evolutionary aspects. Such studies require capture, transport, and short procedures with the fish, some of which might benefit from anesthesia. Currently, either non-anesthetized methods, such as low stress sling capture or immersion anesthesia, are used for most procedures (Fletcher et al., in preparation). While lowering the water level of a tank, and then herding a fish into a vinyl, water-filled sling reduces the stress level of the fish and minimizes any physiological or hematological changes, this technique is only sufficient for simple and painless procedures. Furthermore, anesthetization of a single fish with MS-222 requires either stress-inducing netting of the fish or the time-consuming sling technique. Development of an intramuscular anesthetic technique, which could be delivered via dart. would increase ease of capture and transport of scombrids, while reducing levels of stress page 3 Rollins 1998 and pain experienced by the fish. Moreover, if ketamine/medetomidine anesthesia is shown to not significantly affect hematological parameters of yellowfin tuna, the regimen could be used as an alternative method of obtaining the blood samples necessary for physiological studies. Anesthesia will also benefit research in the field. Immersion anesthetics such as MS-222 cannot be used on individual fish within a noncaptive school without the problems mentioned above. Development of an effective intramuscular agent that can be applied via a dart methodology will allow more extensive investigation of wild populations by enabling insertion of acoustic and archival tags. Likewise, the possibility that blood sampling while under ketamine/medetomidine anesthesia does not significantly bias blood chemistry means that hematological studies could also be performed. While the bonito (Sarda chiliensis) does not have the endothermic capacity of a yellowfin tuna, lacking the extreme capillarization of red muscle that helps to generate elevated temperature, they share the tuna’s high metabolic rate of the tuna (Freund, personal communication). As a scombrid, the bonito is important in comparative studies, serving as a predecessor to the tuna in the evolution of endothermy. Additionally, no baseline blood parameters for the bonito currently exist. The Pacific mackerel, is also a fast-moving scombrid, but lacks the endothermy and the high metabolism of the yellowfin and bonito. This species is also significant from a comparative viewpoint, as an example of a fish closely related to the yellowfin and other tunas, yet preceding the evolution of either elevated metabolism or endothermy. While blood sampling was not possible in the small individuals captured, the development of anesthesia in the species would still serve the same benefit in the capture and transport required by the Tuna Research and Conservation Center (TRCC) in Pacific Grove, CA. Moreover, by comparing the process and behavioral characteristics of anesthesia of all three species, the effects of metabolism and endothermy on anesthesia were able to be ascertained. page 4 Rollins 1998 Preliminary research at the TRCC on yellowfin tuna showed a combination of ketamine hydrochloride and medetomidine could be effective. However, consistent results were not obtained (Block, personal communication). This study was aimed at ascertaining an optimal and repeatable level of anesthesia via a dose response study, while monitoring blood chemistry. Additionally, any variations in anesthetic effectiveness or behavior between the three species of fish were noted. A secondary aim of this study was to determine the extent of the physiological changes resulting from anesthesia. Studies by Fletcher et al. (in preparation) found that variations in capture methodology resulted in differing blood parameters in yellowfin. Specifically, the study found that low-stress level capture via herding into a vinyl sling resulted in much lower hematocrit and hemoglobin than did high-stress capture with a net. Furthermore, plasma levels of alkaline phosphatase (AP), alanine aminotransferase (ALT), aspartate aminotransferase (AST), bilirubin, cholesterol, creatinine, phosphate and potassium were found to be significantly lower in sling-captured yellowfin than in those captured in nets. Anesthesia has also been shown to cause hematological effects similar to net capture in non-scombrid teleosts, such as increased glucose, hematocrit and hemoglobin in different species (Braley and Anderson 1992, Thomas and Robertson 1991, Hseu et al. 1996). These changes are most likely due to activation of the B-adrenergic response by the anesthetic (Houston et al. 1971). This project measured hematocrit, hemoglobin, enzymes, metabolites and electrolytes, and compared the data to the sling-capture data from Fletcher et al. (in preparation). This comparison was performed in order to ascertain the extent of the stress response and following hematological changes resulting from ketamine/medetomidine anesthesia. Ketamine and medetomidine, the main drugs used in the current study, have been used previously, both in nondomestic mammals and in rockfish, and have been found to lead to an anesthesia of good clinical quality (Jalanka 1991 and Williams, personal page 5 Rollins 1998 communication). Medetomidine is an alpha-2-adrenoceptor agonist, inhibiting the activity of adenylyl cyclase, thus reducing signal transduction in the central nervous system (Jalanka 1991). It has strong sedative and analgesic properties, and can be reversed with atipamezole, an alpha-adrenoceptor antagonist and competitive inhibitor of medetomidine (Jalanka 1991). However, used in isolation, medetomidine is not sufficient for general anesthesia (Jalanka 1991). Ketamine is an anesthetic that causes selective, rather than general depression of the CNS (Ryall 1979). Its benefits include rapid induction of and recovery from anesthesia, as well as stimulation of heart rate and cardiac output (Ryall 1979). It is a noncompetitive antagonist of glutamate (NMDA) receptors (Moghaddam et al. 1997). Ketamine also has been shown to have minimal hematological effects in mammals (Hall and Clarke 1983). However, ketamine does not provide sufficient analgesia to allow intrathoracic or visceral surgical procedures (Sawyer 1982). It often increases muscle tension, and also causes hallucinations in humans (Ryall 1979). In combination, ketamine and medetomidine induce a general, short-acting, reversible anesthesia with good sedative and analgesic qualities. This drug combination was chosen partially for its success in previous trials, as well as the benefits of its characteristics. Though intramuscular anesthesia is not currently in use at the TRCC, MS-222 (3¬ amino benzoic acid ethyl ester), a widely used immersion anesthetic, has been used when an anesthetic is required. MS-222, or tricaine, is a water soluble anesthetic agent that is absorbed through the gill surface of a fish. It has been thoroughly studied in several teleost species, including rainbow trout (Gingerich and Drottar 1989, Kebus et al., 1992, Iwama et al., 1989), Atlantic salmon (Hunn and Greer 1991), blacknose dace (MacAvoy and Zaepfel 1997) and red drum (Thomas and Robertson 1991). MS-222 acts by depressing central autonomic functions, and is known to have an asphyxiant effect (Houston et al., 1971) One yellowfin tuna and one bonito were anesthetized using MS- page 6 Rollins 1998 222 and behavioral and physiological effects were monitored, so that MS-222 could be compared and contrasted with the intramuscular anesthesia regimen. Materials and Methods Intramuscular Anesthesia The initial dosage applied in the study was 4 mg/kg ketamine and 0.4 mg/kg medetomidine, and was determined from the preliminary work performed by Williams and Block (personal communication). Atipamezole was always applied in the same dose as medetomidine. Commercial versions of ketamine hydrochloride (Ketasat - Fort Dodge Laboratories, Fort Dodge, IA) and medetomidine (Domitor - Orion, Espoo, Finland) were used, in concentrations of 100 mg/ml and 1 mg/ml in saline, respectively. An experimental version of atipamezole (Wildlife Pharmaceuticals, Fort Collins, CO) was used, in a 5 mg /ml saline solution. Applied doses of the drugs varied from the ideal dose depending on the actual weight of the fish, as well as human error. A partial double dose study was performed (Figure 1). Experimental protocol varied for the three species. For the 5 yellowfin tuna, the water level in the 10 m diameter tank was lowered, and 5 to 7 people entered the tank via ladder. The ladder was then removed. A fish was selected and separated from the school, using a vinyl crowder. The fish was herded into a vinyl sling, filled with water. The curved length of the fish was measured, an approximate weight determined using a length vs. weight chart, and the appropriate volume for the dosage determined. The ketamine/medetomidine combination was injected into the well-vascularized red muscle. A ridge running laterally along the fish was used as a guide to the red muscle, and drugs were injected directly ventral to this ridge, approximately 5 to 10 mm posterior to the pectoral fin. The passive, integrated page 7 Rollins 1998 transponder microchip (or "pit tag") number of the fish was read, a plastic, colored floy tag was inserted for visual identification and the fish was released from the sling. The fish was allowed to swim freely as the anesthetic took effect, with personnel positioned along the walls to prevent the fish from harming itself. Behavioral effects of the anesthesia on the fish were notéd, and when the fish was no longer able to equilibrate, orient and swim independently, it was replaced in the vinyl sling. Forced ventilation of the fish was started, using a submersible pump attached to a hose, which was placed in the mouth of the fish. Once a fish was determined by a lack of muscle tension and motility to be anesthetized, a blood sample was taken, following the method used in Fletcher et al. (In preparation) drawing blood from the bulbus arteriosus. The blood sample was then placed in a vial for hematocrit and hemoglobin analysis, containing heparin (an anticlotting agent), and a vial for plasma separation, containing EGTA (a clotting agent). Samples were then placed on ice until analysis. If the length previously obtained was in question, another measurement was taken at this time. Finally, the dose of atipamezole was measured and injected into the red muscle. The fish remained in the sling under ventilation until it regained a strong tailbeat and showed signs of righting itself and attempting to swim. Upon release, personnel repositioned themselves around the tank, to protect the fish from harm until it regained its orientation and equilibrium. When the fish sufficiently recovered, all personnel left the tank, all equipment was removed, and the water level was restored. Portions of the procedure were recorded using a Sony Hi-8 video camera, and observations of the fish’s condition were made throughout the anesthetic process. Äfter humans left the tank, observations continued to be made approximately every 10 to 15 minutes for approximately 2 to 3 hours. Time between observations continued to increase until the fish died or a week passed, at which point observations were ceased. The 6 bonito and 8 mackerel anesthetized were caught with a baited, barbless hook and line and immediately transferred to a vinyl, water-filled sling held at the edge of the 6 page 8 Rollins 1998 m diameter tank. Weights were estimated based on the relative size of the fish in the tank, and doses were measured as in yellowfin tuna. A pre-determined volume of drug was injected into the red muscle, as guided by the location of the pectoral fin, and the fish was floy tagged. The fish was released and induction of anesthesia was observed. When the fish was determined to be sufficiently anesthetized, the fish was returned to the sling, or netted and then placed in the sling. At this point ventilation was started as before, and a curved length of the fish was taken. Additionally, 3 bonito were weighed, in order to obtain more accurate dosage information. The bonito underwent the same blood sampling procedure as in the tuna; however, mackerel were neither weighed nor was their blood sampled, due to their small size. The predetermined dosage of atipamezole was then injected into the red muscle, and the fish was kept in the sling until an attempt to swim or escape was made. We then released the fish and observed from the side of the tank. Observations followed the same procedure as in yellowfin, but video was not recorded due to lack of assistance. Immersion Anesthesia One yellowfin tuna and one bonito were anesthetized using MS-222. These experiments began with the preparation of the anesthetic bath. A 1 g/L solution of MS- 222 in seawater was used, with a total volume of 30 L. As tricaine causes acidification of seawater, which could lead to undesirable physiological effects in the fish, the drug was buffered with 2 parts sodium bicarbonate per one part MS-222. 30 g of MS-222 and 60 g of sodium bicarbonate were measured and placed in a container holding 30 L of filtered seawater. The solution was then bubbled with an airstone for one hour. 10 L of the bubbled solution were placed in a large cooler and another similarly sized cooler was filled with pure seawater. page 9 Rollins 1998 Fish used for in MS-222 experiments were either netted for yellowfin tuna, or caught with a baited, barbless hook and line for bonito. The fish were placed in a vinyl sling within the MS-222 containing cooler, and the remaining drug solution was poured into the sling. Ventilation of the fish was begun as before. The fish were held in the anesthetic solution for approximately 3 minutes, and were then removed for weighing and measurement of curved length. The fish were then placed in a vinyl sling in the cooler of pure seawater and ventilation was resumed. Blood was then sampled from the bulbus arteriosus. Fish were floy tagged, and when significant movement began, the fish was moved to the tank, but remained ventilated in the sling. Once the fish showed signs of righting and attempting to swim, the fish was released to swim freely in the tank. Observations were made as in the intramuscular procedure, but video was not recorded. Blood Analysis Blood samples were analyzed for hematocrit, placing the heparin treated sample in a standard capillary tube and centrifuging for 5 minutes (5000 rpm), separating red blood cells from white blood cells and blood plasma. The percent of the liquid volume made up by red blood cells was measured, giving a hematocrit level. Hemoglobin was analyzed using a standard preparation (Sigma, St. Louis, MO) and measuring absorbance versus hemoglobin standards using a spectrophotometer at 540 nm. Serum samples were prepared by centrifugation as well, spinning the blood/EGTA-containing vial for 7 minutes (3500 rpm). The separated serum was then analyzed for enzyme and metabolite levels (alkaline phosphatase, aspartate aminotransferase (AST), alanine aminotransferase (ALT), bilirubin, cholesterol, creatine phosphokinase, creatinine and glucose) as well as electrolytes (calcium, chloride, phosphate, potassium and sodium) at the Department of Comparative Medicine at Stanford University. Resulting data from all three measurements were compared to data from Fletcher et al. (in preparation), and were analyzed for statistical significance (two-tailed Student's t-test). page 10 Rollins 1998 Data Analysis Behavioral data were compared to ketamine and medetomidine doses, as well as to the ratio of the two drugs. Stages of anesthesia investigated in the data were: 1. Period of anesthetic induction: defined as time from injection of anesthesia to observation of fish being taken into vinyl sling, as well as being either “out", "under" or otherwise relaxed, with a minimum of movement. 2. Time until release: defined as time from atipamezole injection until release of the fish from the sling. 3. Time until recovery: defined as time from atipamezole injection until fish recovers its orientation and equilibrium skills, as observed by fish avoiding objects in its path and not listing in any direction. 4. Percent survival: defined as number surviving at present; deaths include those attributable directly to anesthesia as well as those due to handling. All averages of anesthetic stages were analyzed as mean, + standard error. Means were then compared using a two-tailed Student's t-test for two means. Averages of blood chemistry values were determined as mean, + standard error. Means between the two sampling methods were compared using a two-tailed Student's t-test for two means of unequal sample sizes. Significance to p + 0.05 was determined by comparing a critical t- value to a test statistic; If the test statistic was greater than the critical value, the means were determined to be significantly different, while if it was less than the critical value, the values were not significantly different. Results Intramuscular Anesthesia page 11 Rollins 1998 The data from individual anesthesia experiments show distinct differences between the three species (Table 1). Average time to anesthesia induction is at a minimum in yellowfin tuna, increases in bonito and is highest in mackerel (Figure 2A). Measurements of time to release in yellowfin are not significantly different from that in bonito. However, mackerel time to release is much less than the other two species, falling to a highly significant minimum (Figure 2B). Though a trend of decreasing time of recovery is apparent, with a maximum in yellowfin and a minimum in mackerel, it is not significant (Figure 2C). The overall percent of anesthetized fish surviving was relatively low in all species, with 0 % survival in yellowfin, followed by mackerel at 38%, and bonito with highest survivorship (50%) (Figure 2D). Analysis of the various anesthetic stages in yellowfin showed no apparent relationship between ketamine dose and time to anesthesia induction, release or percent survival. However, a positive relationship was found between time to recovery and ketamine dose (Figure 3A). No trend was evident in comparing medetomidine dose with time to induction or time to release. Nevertheless, a pattern between time to recovery and medetomidine dose was present, with recovery time decreasing as medetomidine dose increases (Figure 3B). Similarly, while comparisons of induction time or release time versus ketamine:medetomidine ratio showed no trend, a positive trend surfaced in comparison of recovery time to the ratio of the two drugs (Figure 3C). No trends between ketamine dose or medetomidine dose and any of the categories of anesthesia data were apparent in bonito. However, clear trends are evident in all data categories when compared to the ratio of ketamine and medetomidine. In all 3 stages of anesthesia, time measurements decrease with an increase in the ratio (Figure 4A-C). Furthermore, the percentage of bonito surviving decreases significantly as the ketamine: medetomidine ratio increases (Figure 4D). In mackerel, all comparisons of anesthetic data versus individual drug dose gave no patterns or trends. Ratio of ketamine to medetomidine was not analyzed with respect to page 12 Rollins 1998 anesthesia data, as all anesthetized mackerel received the same 5:1 ratio of drugs (Table All three species anesthetized with ketamine and medetomidine displayed the same characteristic behavior patterns. Äfter injection of anesthesia, a fish would begin to increase speed, and fold its pectoral fins against its sides. As the anesthesia took further effect, the fish would lose its equilibrium and orientation ability. The fish then lost its tailbeat and experienced a relaxation of muscle tone in the last stages of induction. Once under anesthesia, the fish would undergo discoloration, which lasted anywhere from several hours to more than a day. Immediately following release, the fish would not be able to orient and equilibrate properly. These skills were regained within 10 to 15 minutes of release. A fish would then enter a hyperexcitable and agitated state, characterized by abnormally high speed, pectoral fins folded against the body, and a general failure to swim with the school. In yellowfin tuna, this state was especially pronounced and the fish never recovered. The agitated state was less severe in bonito, and while it often lasted for at least one day, some of the fish did recover. Mackerel experienced the shortest period of agitation, often returning to a normal swimming pattern within the span of a few hours. Immersion Anesthesia Comparisons of the single yellowfin anesthetized with MS-222 show little difference in time to anesthesia induction; the value of 3.42 minutes (min) is well within the average yellowfin tuna range (mean = 6.73 min; S.D. = 3.50 min; Table 1). Time to release of the MS-222 treated yellowfin is greater than the range for intramuscularly anesthetized yellowfin, with a value of 17.98 min vs. a mean of 6.46 min (S.D. of 6.54 min; Table 1). However, MS-222 measurements of time to recovery give a value within the range of intramuscular values (17.98 min vs. mean = 12.39 min, S.D. = 8.36 min; Table 1). The page 13 Rollins 1998 quality of anesthesia obtained and the recovery of the fish were both qualitatively comparable to that for the ketamine and medetomidine combination. The single bonito anesthetized with MS-222 had a faster anesthesia induction time than the range of values for intramuscularly injected bonito, with a value of 3.43 minutes, versus a mean of 15.91 min (S.D. of 10.36 min; Table 1). Additionally, the times to release and recovery were much longer than the ranges for ketamine and medetomidine anesthesia; release time for MS-222 was 34.23 min, as compared to a mean of 8.81 min (S.D. of 3.71 min), while recovery time for MS-222 was 36.13 min, versus a mean for intramuscular of 11.53 min, (S.D. of 3.65 min; Table 1). The quality of the fish’s recovery was comparable to intramuscular anesthesia, but the quality of the actual anesthesia was much heavier. Blood Chemistry and Hematology Data on blood chemistry and hematological parameters in individual anesthesia experiments are summarized in Table 2. Comparison of hematocrit levels obtained via anesthesia and those obtained from the low-stress sling technique (Fletcher et al., in preparation) are shown in Figure 5, and show no significant difference between the two methods. However, analysis of hematology versus drug dosage in yellowfin shows a significant correlation between increasing hematocrit levels and an increase in the ratio of ketamine to medetomidine (Figure 80). No significant correlations exist in hematology of yellowfin tuna vs. ratio of the two drugs or ketamine dose (Figure 8A and B). In comparing mean enzyme and metabolite values, anesthesia fish had significantly greater values of AST, CPK and cholesterol than in the sling technique (Figure 6). Levels of blood calcium, potassium and sodium were found to be significantly lower in sling technique sampling than anesthesia sampling (Figure 7A-C). However, blood chloride was significantly higher in the sling technique (Figure 7D). Hemoglobin levels were not statistically analyzed due to small sample size. In bonito, a significant correlation was page 14 Rollins 1998 found only between decreasing hematocrit and an increasing ratio of ketamine to medetomidine (Figure 9). All other correlations and parameters in bonito were not analyzed due to small sample size. Discussion Intramuscular Anesthesia Distinct differences in anesthesia induction times were found between the three scombrid species. This correlates with the differences in metabolic rate. The yellowfin, with the highest metabolic rate, would be expected to respond to ketamine and medetomidine most rapidly of the three species. The mackerel, conversely, with the slowest metabolic rate would be expected to have the longest anesthetic induction period. Bonito, with a metabolic rate similar to the yellowfin, but less red muscle capillarization, would be expected to have intermediate induction times. This anticipated pattern is reflected in the minimum induction time found in yellowfin and maximum induction period in mackerel. However, induction time in bonito was not significantly different from that in the yellowfin tuna. This result may be due to the small sample size of the experiments. On the other hand, it is more likely that it reflects the importance of metabolic rate rather than muscle capillarization in anesthetic induction. Despite the differences in the three species' induction time, the data on average time to release seem to contradict a metabolic explanation. The mackerel have an significantly shorter time to release as compared to both bonito and yellowfin. Time to release was defined as the time from injection of atipamezole until the release of the fish from the sling. At this point, the fish showed a regular tailbeat and signs of righting itself, and was also attempting to swim. Subjectivity of this measurement could have contributed to the high variance and the lack of significant difference between time to release of yellowfin page 15 Rollins 1998 tuna and bonito. The minimal times to release in mackerel could mean anesthetic differences result from non-metabolic rate causes. However, the mackerel never fully entered anesthesia, and were actively swimming when recaptured for anesthetic reversal. This could be due to their low metabolic rate. The semi-conscious state of mackerel, therefore, allowed for earlier release, meaning their short release time may be a result of their low metabolism. Though no significant differences were found between the time to recovery in any of the three species, a nonsignificant trend was apparent, with a maximum time for yellowfin tuna and mackerel at a minimum value. The subjectivity inherent in measuring time to recovery, determined as time from atipamezole injection to the time when the fish recovered orientation and equilibrium ability, may have led to the high variance and lack of significance in these values. Additionally, the low sample size may also contribute to the lack of a significant difference. When comparing results in the three species, the fact that the dosages varied somewhat between species and individual fish must be kept in mind. This difference in dosage may confound any conclusions that can be drawn from apparent patterns. However, the difference in species dosages was often due to increasing resistance to anesthesia, as bonito and mackerel were often not sufficiently anesthetized at doses causing rapid induction in yellowfin. The fact that the highest doses were required in the low-metabolizing mackerel, while low doses were effective in the well-vascularized, high metabolizing tuna may reflect effects of metabolism and muscle vascularization on anesthesia. While average anesthesia data from yellowfin tuna is explainable by physiological characteristics, the lack of surviving yellowfin was surprising. Doses of anesthesia in yellowfin may have been too high, leading to observed rapid induction times but harming the fish. However, it is possible that the version of the drugs makes a difference. The differences between isomers of ketamine hydrochloride or medetomidine in the page 16 Rollins 1998 commercial and experimental versions could have caused yellowfin tuna deaths. Experimental versions of ketamine and medetomidine should be applied before viability of anesthesia is determined. In addition, further research into ketamine/medetomidine anesthesia in yellowfin and increased sample sizes may lead to clearer relationships between drug dosages and anesthetic stages. Since developing an ideal anesthetic dose would be the primary goal of any further trials, correlations like those investigated would be highly useful, helping to determine which dose produces the best quality of anesthesia, with the best recovery and rate of survival. In contrast to the yellowfin tuna, anesthesia in bonito appears to be a useful research tool. The encouraging survival rate of bonito, in combination with overall good quality of anesthesia make the ketamine and medetomidine combination an option that should be further investigated, in order to increase sample size and determine correlations between anesthetic stages, percent survival and drug dosage. Though the survival rate and quality of anesthesia in mackerel is not as promising as in bonito, intramuscular anesthesia is still viable. Mackerel agitation level was much higher than in bonito, which led to large amounts of rough handling. Most mackerel made a recovery to near normal behavior before death, but some were found to have severe abrasions from handling. Death, therefore, was most likely due to handling, and if an alternate capturing and restraining procedure is devised, successful anesthesia will be possible. By increasing sample size and lowering death due to handling, the relationship between drugs and anesthetic effects and an ideal ketamine and medetomidine dose will be determined. Immersion Anesthesia In comparing anesthesia with MS-222 versus anesthesia with ketamine and medetomidine, it seems evident that the immersion agent is no better overall than the intramuscular anesthetic. While MS-222 did induce anesthesia more rapidly in bonito, page 17 Rollins 1998 the combination of the increased release and recovery time outweighs any benefit. In yellowfin, the two forms of anesthesia seem quite comparable in every measure, except time to release, in which the ketamine/medetomidine combination is actually preferable, due to its shorter time period. In summation, I feel that the added convenience of an intramuscular anesthesia, in that it can be applied via dart in the wild or captivity, makes it the ketamine/medetomidine regimen preferable to MS-222. Blood Chemistry and Hematology The usefulness of anesthesia is promising, as supported by the lack of a significant difference between hematocrit levels in yellowfin tuna sampling methods. Increases in hematocrit have been shown to be a result of elevated stress in several species of fish (Soivio and Oikara, 1976; Wood et al., 1983; Wells et al., 1984; Railo et al., 1985). Therefore, the absence of any difference between anesthesia and sling hematocrits implies that anesthesia with ketamine and medetomidine does not cause a physiological stress response. While it does appear that hematocrit of yellowfin may be affected by medetomidine increases, the small sample size of this data correlation means that additional research must be performed before any definite conclusions can be drawn. The significant differences in chloride, sodium, potassium and calcium with anesthesia may be attributable to increased stress in the fish. Stress could result in other changes in ionic concentrations, such as the increase in calcium that occurred in this study or the fluctuations in chloride and sodium levels (Fletcher et al., in preparation; Eddy 1981). However, sodium levels would be expected to increase, not decrease as occurred in this study (Eddy 1981). Additionally, a study by Wells et al. showed no increase in sodium or chloride in highly stressed yellowfin tuna (1986). Therefore, the changes in these ions are most likely a result of some other physiological response to anesthesia, or are simply due to the small sample size. The increase in potassium with anesthesia may be a result of stress-released catecholamines causing potassium increases page 18 Rollins 1998 in the blood (Bourne and Cossins 1982). In addition, potassium levels have been shown to increase greatly following increased motor activity (Wood et al., 1983; Soivio and Oikara, 1976). This result correlates, therefore, with the increase in speed noted during the first stages of anesthesia induction. The significant increase in cholesterol between the two sampling techniques is most likely not due to stress, but instead perhaps due to diet differences between the two groups of fish. Aspartate aminotransferase (AST), an enzyme concentrated in the liver (Mommsen 1984), has been shown to increase in stressed, wild yellowfin tuna (Wells et al., 1986). However, the mechanism of such a response is not known (Fletcher et al., in preparation). This means that the increase in AST with ketamine/medetomidine anesthesia is possibly due to stress, but may also result from an unknown cause. However, the increase in creatine phosphokinase (CPK), an enzyme that increases with motor activity (McDonald and Milligan, 1992), also reflects higher level of activity in the anesthetized yellowfin. The highly significant relationship between bonito hematocrit levels and the ratio of ketamine to medetomidine could show an increased stress level with an increased amount of ketamine, relative to medetomidine. However, the small sample size in bonito, in combination with a large range of error, makes the correlation between bonito hematocrit and drug ratio somewhat uncertain. The true effect of anesthetic on bonito hematocrit must be further investigated before any conclusions can be made. Conclusions In conclusion, though the viability of anesthesia in yellowfin tuna seems low, I feel further research should still be performed. The amount of procedural error present in this project, in addition to the small sample size of fish anesthetized, and the lack of investigation into the experimental version makes a final decision on the usefulness of ketamine and medetomidine in yellowfin premature. Furthermore, the lack of change in blood parameters means it remains a good candidate for an alternate blood sampling page 19 Rollins 1998 technique. On the other hand, while viability of the anesthetic regimen in bonito and mackerel seems reasonable, it too needs to be further investigated. Discrepancies in procedural technique need to be eliminated, and an alternate handling method for mackerel must be devised. Additionally, with further studies, the correlation between bonito blood parameters and anesthetic drugs can be better elucidated. This could perhaps add to the promise of this technique in blood sampling, as a baseline bonito blood chemistry could be determined. In all, the limited results of this project should not be viewed as the failure of intramuscular anesthesia in yellowfin tuna, nor should they be regarded as the success of ketamine and medetomidine in bonito or mackerel. Acknowledgments My thanks to Dr. Barbara Block and Dr. Tom Williams for their guidance, assistance and patience. Thanks also to Dr. Heidi Dewar, Ellen Freund, Alexandra Nelson, Tamara Jaron, Andy Seitz, Daniel Dau, Andre Boustany, Simon Fletcher and everyone else who helped out on my project. Dr. Jim Watanabe, thank you for helping me with the statistics on the project. References Bourne, P.K. and A.R. Cossins. On the instability of K+ influx in erythrocytes of the rainbow trout, Salmo gairdneri, and the role of catecholamine hormones in maintaining in vivo influx activity. Journal of Experimental Biology. 101: 93- 104, 1982. Braley, H. and Anderson, T.A. Changes in blood metabolite concentrations in response to repeated capture, anaesthesia and blood sampling in the golden perch, page 20 Rollins 1998 Macquaria ambigua. Comparative Biochemistry and Physiology. 103A(3): 445- 450, 1992. Brill, Richard. On the standard metabolic rates of tropical tunas, including the effects of body size and acute temperature change. Eishery Bulletin. 85: 25-35, 1987. Carey, F.G., Teal, J.M., Kanwisher, J.W. and K.D. Lawson. Warm-bodied fish. American Zoologist. 11: 137-145, 1971. Eddy, F.B. Effects of stress on osmotic and ionic regulation in fish. In Stress and Fish (ed. A.D. Pickering), pp. 11-47. Academic Press, London, 1981. Fletcher, S., E. Freund, T. Williams, H. Dewar, C. Farwell and B.A. Block. Blood sampling in captive yellowfin tuna (Thunnus albacares). in prep, 1998. Gingerich, W.H. and K.R. Drottar. Plasma catecholamine concentrations in rainbow trout (Salmo gairdneri) at rest and after anesthesia and surgery. General and Comparative Endocrinology. 73: 390-397, 1989. Hall, L.W., and K.W. Clarke. Veterinary Anesthesia (eighth edition). Balliere Tindall, London, 1983. Houston, A.H., J.A. Madden, R.J. Woods, and H.M. Miles. Some physiological effects of handling and tricaine methanesulfonate anesthetization upon brook trout, Salvelinus fontinalus. Canadian Journal of Fisheries Research Board. 28: 625- 633, 1971. page 21 Rollins 1998 Hseu, J.R., S.L. Yeh, Y.T. Chu and Y.Y. Ting. Effects of anesthesia with 2- phenoxyethanol on the hematological parameters of four species of marine teleosts. Journal of the Fisheries Society of Taiwan. 23(1): 43-48, 1996. Hunn, J.B. and I.E. Greer. Influence of sampling on the blood chemistry of atlantic salmon. The Progressive Fish-Culturist. 53: 184-187, 1991. Iwama, G.K., J.C. McGeer, and M.P. Pawluk. The effects of five fish anesthetics on acid-base balance, hematocrit, blood gases, cortisol, and adrenaline in rainbow trout. Canadian Journal of Zoology. 67: 2065-2073, 1989. Jalanka, H.H. Medetomidine, Medetomidine-Ketamine Combinations and Atipamezole in Nondomestic Animals: A clinical, physiological and comparative study. Academic Dissertation. College of Veterinary Medicine, Helsinki, Finland, 1991. Lumb, W.V. and E.W. Jones. Veterinary Anesthesia, Second Edition. Lea and Febiger, Philadelphia, 1984. Kebus, M.J., M.T. Collins, M.S. Brownfield, C.H. Amundson, T.B. Kayes, and J.A. Malison. measurement of resting and stress-elevated serum cortisol in rainbow trout Oncorhynchous mykiss in experimental net-pens. Journal of the World Aquaculture Society. 23(1): 83-88, 1992. MacAvoy, S.E. and R.C. Zaepfel. Effects of tricaine methanesulfonate (MS-222) on hematocrit: first field measurements on blacknose dace. Transactions of the American Fisheries Society. 126: 500-503, 1997. page 22 Rollins 1998 McDonald, D.G. and C.L. Milligan. Chemical Properties of the Blood. In Fish Physiology, Vol. 12B (ed. W.S. Hoar, D.J. Randall, and A.P. Farrell), pp. 55-133. Academic Press, San Diego, 1992. Moghaddam, B. B. Adams, A. Verma and D. Daly. Activation of glutamatergic neurotransmission by ketamine: a novel step in the pathway from NMDA receptor blockade to dopaminergic and cognitive disruptions associated with the prefrontal cortex. The Journal of Neuroscience. 17(8): 2921-2927, 1997. Mommsen, T.P. Metabolism of the fish gill. In FEish Physiology, Vol. 10B (ed. W.S. Hoar, D.J. Randall, and A.P. Farrell), pp. 203-238. Academic Press, San Diego, 1992. Railo, E., Nikinmaa, M., and Soivio, A. Effects of sampling on blood parameters in rainbow trout, Salmo gairdneri: richardson. Journal of Fish Biology. 26: 725- 732, 1985. Ryall, R.W. Mechanisms of Drug Action on the Nervous System. pp. 70. Cambridge University Press, Cambridge, 1979. Sawyer, D.C. The Practice of Small Animal Anesthesia. W.B. Saunders Co., Philadelphia, 1982. Soivio, A. and A. Oikari. Haemotological effects of stress on a teleost, Esox lucius. Journal of Fish Biology. 8: 397-411, 1976. page 23 Rollins 1998 Thomas, P. and L. Robertson. Plasma cortisol and glucose stress response of red drum (Sciaenops ocellatus) to handling and shallow water stressors and anesthesia with MS-222, quinaldine sulfate and metomidate. Aquaculture. 96: 69-86, 1991. Wells, R.M.G., et al. Recovery from stress following capture and anesthesia of Antarctic fish: hematology and blood chemistry. Journal of Fish Biology. 25: 567-576. 1984. Wells, R.M.G., R.H. Mclntyre, A.K. Morgan and P.S. Davie. Physiological stress responses in big gamefish after capture: observations on plasma chemistry and blood factors. Comparative Biochemistry and Physiology. 84A: 565-571, 1986. Wood, C.M., Turner, J.D., and M.S. Graham. Why do fish die after severe exercise? Journal of Eish Biology. 22:189-201, 1983. page 24 Rollins 1998 Figure Legends Figure 1: The figure shows the design of the double dose study that was only partially completed due to mortality. Medetomidine doses are along the top and ketamine doses are along the side. (B) indicates that the dose was applied to a bonito; (Y) indicates a dose was applied to a yellowfin tuna; (M) indicates a dose was applied to a mackerel. Figure 2: The panel shows averages of induction period (A), time to release (B), time to recovery (C), as well as survivorship (D) for yellowfin tuna, bonito and mackerel. Standard error bars are included in the three graphs of time vs. species. Figure 3: The panel shows the time until recovery in yellowfin tuna, as compared to ketamine dose (A), medetomidine dose (B) and the ratio of ketamine to medetomidine (C. Standard error bars are included only where the value given is an average. Time is along the y-axis, while drug or drug ratio is along the x-axis. Figure 4: The panel gives the average of time of induction, time until release, time until recovery and survivorship versus the ratio of ketamine to medetomidine for bonito. Where the average is based on a sample size of greater than one, standard error bars are included. Time is along the y-axis, and the drug ratio is along the x-axis. Figure 5: This figure shows the average hematocrit of yellowfin tuna, versus which sampling method was used. The sampling methods are along the x-axis, and are anesthesia with ketamine and medetomidine, or the low-stress sling technique. Hematocrit is measured along the y-axis. Values are presented as means, with standard error bars. Sample size for anesthesia is 5, and is 24 for the sling method. page 25 Rollins 1998 Figure 6: This panel measures the amount of alanine aminotransferase (A), creatine phosphokinase (B) and cholesterol (C) versus blood sampling method in yellowfin tuna. Sampling methods are anesthesia (left) and sling technique (right), and run along the x¬ axis. Figure 7: This panel shows the level of calcium (A), chloride (B), potassium (C) and sodium (D) versus sampling method in yellowfin tuna. Sampling methods are anesthesia (left) and sling technique (right) along the x-axis. Figure 8: This panel gives the relationship between yellowfin tuna hematocrit, and either ratio of ketamine to medetomidine (A), ketamine dose (B) or medetomidine dose (C). Ratios or drug dosages run along the x-axis, while hematocrit is on the y-axis. For Figure 8A, the regression line equation is y = -1.04x + 39.45 and R2 = 0.64. For Figure 8B, the equation is y = -2.28x + 40.22 and R2 = 0.28. In Figure 8C, y = 52.67X + 8.65 and R2 = 0.83. Figure 9: This panel gives the relationship of bonito hematocrit and either ratio of ketamine to medetomidine (A), ketamine dose (B) or medetomidine dose (C). Ratios or drug doses are on the x-axis, while hematocrit is on the y-axis. In Figure 9A, the regression line equation is y =-0.94x + 32.4 with an R2 = 1. For Figure 9B, y =-4.50x + 38.61, and R2 = 0.50. In Figure 9C, y =-21.21x + 37.85 and R2 =0.44. page 26 Table 1. Summary of Anesthesia: Part I - Yellowfin Tuna Time to Ratio of Ketamine Anesthesia Time to Dose Medetomidine ketamine: Release Species and Induction weight (kg)' (mgkg) Dose (mgkg) medetomidine (min) (min) Yellowfin 7.5 4.8 (7.3) 0.38 10.8:1 Yellowfin (10)* 0.42 3.1:1 Yellowfin (9)* 0.44 17.9 9.1:1 2.7 Yellowfin 0.51 5:1 3.6 4.1 2.53 (5.9) Yellowfin 10.6 1.5 (4.6) 3.02 0.604 5:1 1gMS¬ Yellowfin MS-222 222/L n/a 3.4 18 (6.1) seawater n/a = estimated weight page 27 Time to Recovery (min) 18.9 na 20.2 6.6 3.9 Comments and time of death (after anesthesia injection) good anesthesia, died (Q 3 hours, 50 minutes good anesthesia; underwent fright response and never recovered; euthanised + 59 minutes, 53 seconds good anesthesia; died by 21 hours good anesthesia; died (Q 25 hours, 46 minutes good anesthesia; died (Q 10 hours, 35 minutes good anesthesia; decent recovery; euthanised for research by 144 hours Table 1. Summary of Anesthesia: Part II - Bonito Time to Ketamine Ratio of Anesthesia Time to Species and Dose Medetomidine ketamine: Release Induction weight (kg)t (mgkg) Dose (mgkg) medetomidine (min) (min) 5.5 2.7 Bonito (2.0) 0.4 10:1 1.4 0.28 5:1 8.1 6.5 Bonito (3.2) Bonito (2.8) 15.5 13.7 1.82 0.36 5:1 2 0.4 5:1 22.1 11 Bonito (2.6) 12.8 7.8 Bonito (1.7) 0.6 5:1 Bonito 0.8 5:1 33 9.7 (2.5) 1gMS¬ Bonito- MS-222 222/L n/a 3.4 34.2 seawater n/a (2.6) * = estimated weight page 28 Time to Comments and time of Recovery death (after anesthesia injection) (min) good anesthesia; jumped out of tank; died by 17 hours, 30 minutes good anesthesia and 8.9 recovery; survived good anesthesia; long recovery due to injury; 14.3 survived anesthesia not induced; fell on floor; died by 20 hours, 32 minutes 16.3 light anesthesia; died 7.8 by 17 hours, 12 minutes light anesthesia; slow recovery but survived 13.7 anesthesia too heavy; died by 42 hours; very abraded 36.1 Table 1. Summary of Anesthesia: Part III - Pacific Mackerel Time to Ketamine Ratio of Anesthesia Species and Dose Medetomidine ketamine: Induction length (kg) (mgkg) Dose (mgkg) medetomidine (min) Mackerel (0.75) 0.4 5:1 n/a Mackerel (0.75)* unknown unknown n/a na Mackerel 6.55 1.31 5:1 (0.6) 21 Mackerel 3.58 0.72 23.2 (1.1) Mackerel 0.8 (0.5)* Mackerel 0.77 3.84 5:1 60.2 (1.3) Mackerel (0.5) 5:1 24.3 Mackerel 1.39 6.94 5:1 40.1 (0.7) * = estimated weight page 29 Time to Release (min) n/a n/a 1.3 Time to Recovery (min) n/a n/a 27.4 Comments and time of death (after anesthesia injection) anesthesia never induced or reversed; survival unknown injection mistake; anesthesia not induced or reversed; survival unknown light anesthesia; bad recovery; euthanised by 2 hours, 42 minutes light anesthesia; good recovery but euthanised (Q 50 hours, 5 minutes light anesthesia; good recovery; survived light anesthesia; good recovery; died by 5 hours; very abraded light anesthesia; good recovery; survived light anesthesia; good recovery; died by 55 hours, 47 minutes; very abraded Table 2. Summary of Blood Chemistry: Part I - Hematocrit and Hemoglobin Ratio of Hematocrit Ketamine Medetomidine ketamine to (% red Hemoglobin Species and Dose Weight (kg) (mgkg) Dose (mgkg) medetomidine blood cells) (gdL blood) Yellowfin 0.38 10.8 to 1 27.5 na (7.3) Yellowfin (10)* 1.3 0.42 3.1 to 1 33,5 n/a Yellowfin 0.44 9.1 to 1 29.5 11 Yellowfin 2.53 5to 1 37 15.58 0.51 (5.9) Yellowfin 5 to 1 39.5 16.32 0.604 3.02 (4.6) 1 gMS¬ Yellowfin- 222 n/a 22 n/a MS-222 (6.1) L seawater n/a 23 n/a 10 to 1 Bonito (2.0) 0.28 5 to 1 n/a 32.5 Bonito (3.2) 15.53 5 to 1 36.5 0.36 Bonito (2.8) 1.82 11.28 25 5 to 1 Bonito (2.6) 9.63 20.5 0.6 5 to 1 Bonito (1.7) Bonito (2.5) 9.23 0.8 5 to 1 24 1 gMS¬ Bonito- 222/ 40 n/a n/a MS-222 (2.6) L seawater n/a * = estimated weight page 30 Table 2. Summary of Blood Chemistry: Part II - Enzymes and Metabolites Species and AST Bilirubin Cholesterol CPK Creatinine Glucose Weight (g) QUL) ALTQUD) APGUA)(mgd)(mgd) (UT)(mgd) (mgd) Yellowfin 123 183 0.3 107 (7.3) Yellowfin (10)* 187 1111 0.2 92 Yellowfin (9)* 137 884 0.2 78 Yellowfin (5.9) 186 1244 0.2 121 Yellowfin 0 126 1306 25 108 (4.6) Yellowfin- 90 297 888 0.3 129 MS-222 (6.1) 239 109 0.3 192 Bonito (2.8) 260 143 0.3 102 Bonito (1.7) 0.3 219 282 180 Bonito (2.5) * = estimated weight page 31 Table 2. Summary of Blood Chemistry: Part III - Electrolytes Species and Chloride Phosphorus Potassium Calcium Sodium Weight (g) (mgd) (meql) (mgd) (meqL) (meqL) Yellowfin 168 5.4 2.5 14.2 210 (7.3) Yellowfin (10) 168 210 14.2 5.4 2.5 Yellowfin (9)* 14.6 197 165 5.2 3.4 Yellowfin 203 13.7 166 (5.9) 3.1 Yellowfin 166 2.8 (4.6) 14.6 203 Yellowfin - MS-222 (6.1) 18.1 207 4.7 6.2 232 15.6 4.3 184 Bonito (2.8) 149 6.4 169 3.2 206 Bonito (1.7) 16.6 191 3 Bonito (2.5) 11.5 4.3 154 * = estimated weight page 32 Figure 1- Double Dose Study Model Medetomidine 0.8 mgkg 0.4 mgkg 0.1 mgkg 0.2 mgkg medetomidine medetomidine medetomidine medetomidine 1 mgkg ketamine Ketamine B 2 mgkg ketamine 4 mgkg ketamine Y, B B.M 8 mgkg ketamine Y = applied to yellowfin tuna B = applied to bonito M = applied to mackerel page 33 Figure 2 — A. Induction Bono Species C. Recover Species uades B. Release Velonin Tuna Bonto Species D. Survivorship Veloufn Tuna Bonito Species Mackel naen page 34 Figure 3 A. Recovery vs. Ketamine Dose Ketamine Dose (mg/kg) B. Recovery vs. Medetomidine Dose Medetomidine Dose (mg/kg) C. Recovery vs. Ketamine to Medetomidine Ratio 0 9.1 11:1 3:1 Ketamine to Medetomidine Ratio page 35 0. Figur A. Induction vs. Ketamine to Medetomidine Ratic B. Release vs. Ketamine to Medetomidine Ratio Ketamine to Medetomidine Ratio Ketamine to Medetomidine Ratio C. Recovery vs. Ketamine to Medetomidine Ratio D. Survivorship vs. Ketamine to Medetomidine Ratio 10.1 101 Ketamine to Medetomidine Ratio Ketamine to Medetomidine Ratio page 36 Figure 5 35 - 20 10 anesthesia Sampling Method page 37 sling Figure 6 20 eingnetaes Method of Sampling Anonenes Method of Sampling sing method Method of Sampling page 38 c. sing method Sampling Method anestese sing method Sampling Method anstesa sing method Sampling Method sing mehos Sampling Method Figui page 39 Figure 8 30 30 2 Ketamine to Medetomidine Ratio (x:1) Ketamine Dose (mgkg) 0.40 0.45 0.50 0.55 0.60 0.65 Medetomidine Dose (mg/kg) page 40 Figure A. 38 10 11 Ketamine to Medetomidine Ratio (x:1) Ketamine Dose (mg/kg) 02 03 04 05 0.6 0.7 0.8 0.9 Medetomidine Dose (mg/kg) page 41