Abstract: Zebrafish, Danio rerio, are a useful model system for vertebrate cardiovascular research. Their transparent bodies during the larval stage of development allow for in vivo experimentation. Pharmacological experimentation reveals important similarities between zebrafish hearts and those of mammals. Muscarinic cholinergic receptor activity was demonstrated through the dose dependent decrease in heart rate caused by the acetylcholine analog carbachol. Adrenergic receptor responses were elicited by norepinephrine and isoproterenol. The inhibition of intracellular calcium release channels by ryanodine also had a decelerating effect on heart rate, as did the disruption of sodium-potassium active pumps by ouabain. The stimulation of an undefined nitric oxide pathway by two nitric oxide donors also slowed heart rate. Clearly, the pharmacologic responses of the zebrafish heart should be further explored as a model for vertebrate cardiovascular physiology and as a foundation for research in the genetics and cardiovascular development of zebrafish. Introduction Danio rerio, commonly known as zebrafish, are fresh water tropical fish that naturally occur in India. Zebrafish are used for biological research due to their short generation time, the relative ease of their maintenance, their sufficiently small body size permitting the storage of large populations. The defining characteristic that sets them apart from other potential vertebrate model systems is that their bodies in the larval stage are transparent. Their transparency allows for detailed observations of the cardiovascular system in vivo without the complications of surgical procedures. I began studying the zebrafish cardiovascular system with the goal of studying vascular development, growth and repair. Technical problems with this goal included the difficulty in obtaining cross-reacting mammalian antibodies to receptors and to endothelial cell growth factors and the lack of a visible response to certain pharmacological agents that have been shown to play a role in the vascular actions of other model systems. The size of zebrafish, while allowing for easy storage, made controlled wounding extremely difficult. These problems highlighted the need for more knowledge describing the cardiovascular physiology of the normal zebrafish. The short generation time and transparent bodies of the zebrafish caused the fields of genetics and developmental biology to be interested in zebrafish as a model system to study cardiovascular mutations among others. However, before abnormal zebrafish hearts can be characterized, better understanding of the normal zebrafish heart is needed. The zebrafish heart has developed two distinct chambers before the larva hatches (Kimmel 255). Heart beat developes even sooner, within 24 hours of fertilization. Vasodilation, vasoconstriction, changes in stroke volume, changes in heart rate are essential actions of vertebrate cardiovascular systems allowing response to stimuli. These processes can be witnessed in vivo in zebrafish hearts through stimulation of muscarinic cholinergic receptors, adrenergic receptors, intracellular calcium pathways, sodium-potassium active pumps, and nitric oxide pathways. The hypothesis of this project was that it would be possible to examine the muscarinic cholinergic and adrenergic receptor activity and the intracellular pathways of the larval zebrafish heart through manipulation with known pharmacological agents. Cholinergic receptors are responsible for actions of the parasympathetic system. They include both nicotinic and muscarinic receptors. To activate these receptors an acetylcholine analog, carbachol, was used. To control for the fact that muscarinic rather than nicotinic receptors were being activated, Curare was used as an immobilizer to keep the fish in place and also as an inhibitor of nicotinic receptors. Adrenergic receptors are part of the sympathetic system. Fish have been shown to have such receptors and respond to adrenaline and norepinephrine but with less increase in heart rate than expected by mammals (Satchell 162). Norepinephrine activates both alpha and Bi adrenergic receptors, while isoproterenol only activates beta receptors (Katzung 127-128). The pharamacological agent Ryanodine inhibits ryanodine receptors necessary in the intracellular release of Calcium into the cytosol. It is clinically used to treat the excessive release of calcium from the sarcoplasmic reticulum that may result in the fatal condition of malignant hyperthermia (Taylor 188). Calcium is needed to although cardiac cells to contract properly. In addition to inhibition of ryanodine receptors by ryanodine, intracellular sodium potassium active pumps were inhibited by ouabain. As a cardiac glycoside, it inhibits the natural exchange of sodium and potassium and causes the cells to lose potassium and accumulate calcium (Kelly and Smith 814). Thus the cells become depolarized. The role of nitric oxide in relation to heart rate was explored using to nitric oxide donors, Spermine NONOate and S-nitroso-N-acetylpenicillamine (SNAP). Spermine NONOate releases higher levels of nitric oxide but its release period is shorter than that of SNAP (Shih 12). SNAP releases low levels of nitric oxide for a considerable time period. Materials and Methods Adult zebrafish were maintained in fresh water at 28° Celsius, under a controlled light source with a regular light cycle of 9 dark hours in a 24 hour period. In order to obtain fertilized eggs, marbles were placed in the tank the night before. I then syphoned the bottom of the tank in the morning and manually separated the fertilized eggs. Next, I placed the eggs in 10% normal hanks and 90% de-ionized water solution in an incubator at 28° Celsius. Larvae between 6 and 8 days post fertilization were used for each experiment. I immobilized each larva with 2 mg d-Tubocurarine in 1 ml 10% Hanks solution. The larvae were placed in a temperature controlled stage of the light microscope at 28 Celsius. A robotic arm was used to inject all the pharmacological agents except NONOate through a glass capillary tube directly into the caudal end of the pericardium. luM Carbachol, 100 uM Isoproterenol,100 uM norepinephrine, 200 uM SNAP, 1 uM Quabain, and 100 uM Ryanodine were the concentrations injected. NONOate was added to the diluted Hank solution surrounding the larva to a final concentration of 100 UM, instead of injection. Vacuum grease helped secure the larva in the same place on the slide. All injections were made at a pressure of 60 psi. Each injection and reaction was observed under a magnification of 10 with Nomarski optics and videotaped. We digitized the heart rate from the visual data of the video tape by using a light sensor and the computer program Dempster. The interpeak interval, or period, was measured using this program. The heart beat is the frequency, or inverse of the period, converted to beats per minute. The control for each experiment was a baseline reading of that particular larva’s heart beat and circulation before the administration of the pharmaceutical agent. In addition to these individual controls, I recorded larval heart beat under anesthesia by luM MS 222, to control for the effects of d-Tubocurarine. A control was needed for d- Tubocurarine because it is a vasodilator and it releases histamine (Taylor 187). Results There were no clear differences between the average heart rate of six larvae immobilized by Curare and one anesthetized by MS 222 (212 bpm and 189 bpm respectively as illustrated in figure 1). Figure 2A comprises the raw data obtained from the light sensor for carbachol. Carbachol demonstrated a dose dependent deceleration of heart rate. The heart rate of larval zebrafish increased in response to 100 uM isoproterenol and 100 uM norepinephrine, with a greater increase in response to isoproterenol (Figure 3). The acceleration in response to norepinephrine reached a plateau at approximately 220 bpm even with further doses of norepinephrine (Figure 4). Both nitric oxide donors decreased the heart rate. Within 15 minutes of injection of 200 uM SNAP, the heart rate had decreased by half its original rate (Figure 5). Within the same time period of 15 minutes, NONOate had less of an effect on heart rate (decreasing it by 40 beats per minute) than SNAP did (decreasing it by 140 beats per minute) (Figure 6). Overall, SNAP decreased heart rate much more dramatically then NONOate (Figure 7). Within 12 minutes, 100 uM ryanodine decreased the heart rate from 212 beats per minute to 89 beats per minute (Figure 8). Increasing doses of 1 uM ouabain slowed the heart rate from 216 beats per minute to 82 beats per minute. In addition to the change in heart rate, the standard deviation of heart rate is a measurement of cardiac arrhythmia. Ryanodine, both nitric oxide donors, and oubain caused profound cardiac arrhythmia. However, ryanodine caused the most dramatic arrhythmia (Figure 10). The maximum standard deviation of ryanodine was 472. The standard deviation is a slightly misleading measurement of arrhythmia however because the data are skewed heavily to the side o slower heart rates; the major arrhythmias were all long pauses in heart rate rather than irregular accelerations. Figure 11 shows the raw data from a portion of the ryanodine experiment, including two long pauses in heart rate. Discussion The difference in the degree to which both nitric oxide donors decreased the heart rate could be due to the procedure of bathing the larva with NONOate rather than directly injecting it into the pericardium. Another possible reason for this difference could be the differences in concentration. NONOate had been expected to release more nitric oxide than SNAP. Both carbachol and the nitric oxide donors dramatically slowed the heart rate. Further experimentation is needed to show the relation, if any, between the activation of muscarinic cholinergic receptors and the nitric oxide pathway. In a 1996 study by Feldman et. al., the muscarinic cholinergic receptors in rats that were involved in increases in heart rate were linked to a nitric oxide production pathway by experimentation that inhibited this cardiac acceleration by the application of nitric oxide inhibitors L-NAME and Methylene blue (21 1). Now that both nitric oxide and carbachol show acceleration in zebrafish heart rate, important further experimentation includes manipulation with nitric oxide inhibitors. Another important test of the stimulatory action of muscarinic cholinergic receptors by carbachol would be to block such stimulation with atropine. This manipulation could be combined with nitric oxide donors to see if artificial activation of the nitric oxide pathway down stream was enough to overcome the inhibition of the proposed pathway upstream. An important component of future experiments would be to compare light sensor information from different regions of the heart because Davies et. al. states that cholinergic innervation only occurs in the fish atrium not the ventricle (261). The actual reaction of the heart to the catecholamines was more than the expected one. Fish heart rates are expected to increase “15-20% compared with the 100% increase reported in some mammals" (Satchell 162). Although the direct effect of norepinephrine in humans is an accelerated heart rate, the culmination of effects is often a slowed heart rate because of the compensatory mechanisms. In the case of larval zebrafish, these compensatory mechanisms were not detected. The effect may be masked by part of the experiment's design: increasing doses of norepinephrine were added (Figure 4). We believed the multiple doses would not have an additive effect because of the short time period of the drug’s action. However, the increase in dose caused by the increase in duration may have overcome the body’s compensatory mechanisms. The extremely rapid heart rate of more than 220 beats per minute may be possible only in these larval fish. Fetal mammals have a faster heart rate than that of adult mammals of the same species. The response to catecholamines may be mediated through increases in calcium flow within the contractile mechanisms of the cardiac cell (Satchell 162). This idea is supported by the changes in heart rate and rhythm pattern caused by ryanodine. Ryanodine produced not only a dramatically slower heart rate, but also large standard deviations in this rate. These arrhythmias may be caused by the dramatically slowed rate and the need (according to Starling’s Law) for the heart to be sufficiently full and the cardiac muscle thus sufficiently stretched, before the heart can contract. In fact, calcium is the molecule responsible for contraction of cardiac cells in relation to Starling’s law because cardiac muscles are more sensitive to being stretched because the troponin in cardiac muscle cells is more likely to bind to calcium than is other muscle troponin (Satchell 38). Calcium may also contribute to the change in rhythm not only because of this difference of the affinity of cardiac cell fibers for calcium, but also in some other mechanism. Calcium plays a role in the regular rhythm of the vasomotion of arteries, and ryanodine can inhibit that role (Griffith and Edwards H1696). The data collected by ryanodine is surprising for a teleost because previous studies argued that extracellular rather than intracellular sources of calcium played more prominent roles (Vornanen R1432). Bradykinin, verapamil, and diltiazem have been used to show differences in the roles of extracellular and intracellular calcium sources in canine cells and should be used in future experimentation to explore the role of calcium in the zebrafish heart (Yang et. al. 59). Quabain's mode of action was to disrupt the active exchange of sodium and potassium. Theoretically as a cardiac glucoside, ouabain should have contributed to an increase in intracellular calcium and thus had opposite effects of ryanodine’s inhibition of intracellular release of calcium. A study by Gjini, et. al. show that a cardiac glucosides reduce the calcium current (95). A reduction in calcium current could have had similar effects as an inhibition of calcium release, thus explaining the similar responses to ryanodine and ouabain. A significant next step in this research will be to apply the tool of the light sensor to examine perfusion rates and quantify vasoconstriction and vasodilation. Nitric oxide is a vasodilator (Eckenhoff and Longnecker 356). Histamine which may be stimulated by Curare is also a vasodilator (although the control showed it did not exhibit clear contributions) (Babe and Serafin 585). The light sensor technique will be especially important with pharmacological agents like norepinephrine that act as vasoconstrictors in many areas of the body while acting as vasodilators in the heart muscle. It will help compare norepinephrine’s effects to those of the vasodilator isoproterenol. Discuss problems with model?? Such as the fact that an important hypoxia response is the coupling of cardiac and respiratory rate. Since larval fish 'respirate" through absorption through the skin rather than gill tissue or lungs, the mechanisms are so different that the coupling response is not seen Satchell 172. Suggest another pathway to explore? There are many interesting articles on the role of adenosine and the response of the AV node including Dennis, DM et. al. 1995. And in comparison with carbachol (Koglin, J 1994) Conclusions Through manipulation by pharmacological agents, these experiments support the hypothesis that the larval zebrafish heart has muscarinic cholinergic receptor activity, adrenergic receptor activity, an intracellular calcium release pathway necessary for proper contraction, and a nitric oxide pathway necessary for normal rhythm similar to that of mammals. Therefore zebrafish are an effective vertebrate model system for cardiovascular research. Further experimentation with the vascular responses to these pharmacological agents is needed, and the transparency of the larval zebrafish bodies will allow for a new technique of data collection on cardiovascular physiology by a light sensor. Literature Cited Babe, Kenneth S. and Serafin, William E. "Histamine, Bradykinin, and Their Antagonists." The Pharmacological Basis of Therapeutics. New York: McGraw Hill Inc.; 1996; 581-600. Davies, Philip J., Donald, John A., & Campbell, Graeme. "The distribution and colocalization of neuropeptides in fish cardiac neurons.” Journal of the Autonomic Nervous System 46. 1994; 261-272. Eckenhoff, Roderic G. and Longnecker, David, E. "The therapeutic gases." Goodman and Gilman's The Pharmacological Basis of Therapeutics. New York: McGraw Hill Inc.; 1996; 349-359. Feldman, D. S.; Terry, A.V.; and Buccafusco, J. J.. "Spinal muscarinic and nitric oxide systems in cardiovascular regulation." European Journal of Pharmacology 313(3); October 1996; 211-220. Gjini, V. et. al. Frequency dependence in the action of the class III antiarrhythmic drug dofetilide is modulated by altering L-type calcium current and digitalis glucoside. Journal of Cardiovascular Pharmacology 3 1(1); January 1997; 95-100. Griffith, T. M. and Edwards, D. H. "Calcium sequestration as a determinant of chaos and mixed-mode dynamics in agonist-induced vasomotion." American Journal of Physiology (272(4(2)) April 1997; H1696-H1709. Katzung, Bertram, ed. Basic and Clinical Pharmacology. Stamford, Connecticut: Appleton and Lange; 1998. Kelly, Ralph A. and Smith, Thomas W. "Pharmacological Treatment of Heart Failure. Goodman and Gilman's The Pharmacological Basis of Therapeutics New York: McGraw Hill Inc.; 1996; 809-839. Kimmel, Charles, et. al. "Stages of embryonic development of the Zebrafish. Developmental Dynamics 202; 1995; 253-310. Satchell, George. Physiology and Form of Fish Circulation. Cambridge: Cambridge University Press; 1991. Shih, Karen. "Nitric Oxide Promotes while Cholinergic Agonist and Cyclic GMP Inhibit Neurite Outgrowth of NIE-115 Mouse Neuroblastoma Cells." Pacific Grove, California: Hopkins Spring Class 1997 Papers. Taylor, Palmer. "Agents acting at the nueromuscular junction and autonomic ganglia. Goodman and Gilman's The Pharmacological Basis of Therapeutics. New York: McGraw Hill Inc.; 1996; 177-197. Vornanen, Matti. "Sarcolemmal Ca influx through L-type Ca channels in ventricular myocytes of a teleost fish." The American Physiological Society. 1997; R1432- R1440. Yang, CM. et. al. "Bradykinin-stimulated calcium mobilization in cultured canine tracheal smooth muscle cells." Cell Calcium 2; August 1994; 59-70. Acknowledgements: I would like to thank Dr. Stuart Thompson and Dr. Adawia Alousi for their incredible dedication, instruction, and guidance. It has been an honor to work with them. I would also like to thank Christian Riley and Matt McFarlane for their continual support and patient answers to my questions. Figure Legend For all figures, the error bars represent standard deviations in heart rate Figure 1. Although the average larval heart rate under Curare is slightly higher (212 beats per minute) than that under MS 222 (190 beats per minute), there is no clear difference between them. Figure 2 A is a collection of raw data collected from the light sensor on the response to carbachol: The amplitude merely reflects the change in optical density of the sample site and is thus unimportant. As the dose is increased through a longer duration of the pulse of injection, the interval between contractions increased. B: The increase of this interval was then normalized with respect to the actual dose in picoliters. The actual dose was calculated by injecting different durations of pulses into oil. There is a clear dose dependent negative response of heart rate to Carbachol. Figure 3. The heart rate increased in response to norepinephrine by 20 beats per minute. It increased by approximately 30 beats per minute. Figure 4. Increased injections of 100 uM Norepinephrine did not dramatically increase the response of the heart. Figure 5: Within 15 minutes of injection of 200 uM SNAP, heart rate decreased by 50%. Figure 6. Within 15 minutes of administration of 100 uM NONOate, heart rate decreased By 40 beats per minute. Figure 7. Administration of 200 uM SNAP decreased the heart rate more than that of 100(M NONOate. Figure 8. Following the injection of 100 uM ryanodine, the heart rate decreased from 212 beats per minute to 89 beats per minute. Figure 9. Increasing injections of ouabain decelerated the heart rate even more. Figure 10. The decrease in heart rate after injection of 100 uM ryanodine was dramatic and continual. The huge standard deviations (as illustrated by large error bars) at different sampling periods show cardiac arrhythmia. Figure 11. Four beats into this sequence, there is a larger interval between peaks. It represents a pause between heart beats. The heart recovers to normal and then there is an even more dramatic pause between contractions of a couple of seconds. 300 250 200 150 100 Figure 1. Control Curari MS 222 Immobilized & Anesthetized Figure 2: Carbachol: raw data and dose response curve A 50ms 150 300 400 veeeete 500 B 2.0 - 1.8 1.6 1.4 1.2 1.0 % 0.0 0.5 10sec 1.5 2.0 CCh injection (pl) delta OD 250 200 150 - Figure 3: Adrenergic Receptor Agonists . NE Control Control Isoproterenol NE 300 200 100 40 ms 40 ms Figure 4: Norepinephrine 80 ms 120 ms Time (min.) 250 ms 20 300 200 100 200 microM SNAP Figure 5: SNAP Time (min.) 20 25 300 200 100 - 100micron NONOate 0 Figure 6: NONOate 2 4 6 8 10 12 14 16 18 time (min.) 200 100 S Control Figure 7: Nitric Oxide Donors N Control SNAP NONOate 350 300 250 200 150 100 Figure 8: Inhibitor of Intracellular Ca Release Channels ... Ryanodine Control 300 200 10 Figure 9: Quabain 50 ms 150 ms 350 ms Time (min.) 450 ms 15 20 500 400 3 300 200 100 Figure 10: Ryanodine I 50ms pulses of 100microM Ryanodine 2 8 Time (min.) 28 10 12 14 Figure 11: A section of raw data from a ryanodine experiment 5 sec